4-Ethyl-1-[4-(methyl­sulfan­yl)benzyl­idene]thio­semicarbazide

There are four independent mol­ecules in the asymmetric unit of the title compound, C(11)H(15)N(3)S(2), with different conformations: the dihedral angles between the benzene rings and thio­urea units are 16.85 (9), 0.56 (10), 8.05 (12) and 4.56 (8)°. Each mol­ecule contains an intra­molecular N—H⋯N...

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Detalles Bibliográficos
Autores principales: Li, Yu-Feng, Jian, Fang-Fang
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3006876/
https://www.ncbi.nlm.nih.gov/pubmed/21587932
http://dx.doi.org/10.1107/S1600536810022920
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author Li, Yu-Feng
Jian, Fang-Fang
author_facet Li, Yu-Feng
Jian, Fang-Fang
author_sort Li, Yu-Feng
collection PubMed
description There are four independent mol­ecules in the asymmetric unit of the title compound, C(11)H(15)N(3)S(2), with different conformations: the dihedral angles between the benzene rings and thio­urea units are 16.85 (9), 0.56 (10), 8.05 (12) and 4.56 (8)°. Each mol­ecule contains an intra­molecular N—H⋯N hydrogen bond, generating an S(5) ring. The crystal structure is stabilized by inter­molecular N—H⋯S hydrogen bonds.
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spelling pubmed-30068762010-12-30 4-Ethyl-1-[4-(methyl­sulfan­yl)benzyl­idene]thio­semicarbazide Li, Yu-Feng Jian, Fang-Fang Acta Crystallogr Sect E Struct Rep Online Organic Papers There are four independent mol­ecules in the asymmetric unit of the title compound, C(11)H(15)N(3)S(2), with different conformations: the dihedral angles between the benzene rings and thio­urea units are 16.85 (9), 0.56 (10), 8.05 (12) and 4.56 (8)°. Each mol­ecule contains an intra­molecular N—H⋯N hydrogen bond, generating an S(5) ring. The crystal structure is stabilized by inter­molecular N—H⋯S hydrogen bonds. International Union of Crystallography 2010-06-18 /pmc/articles/PMC3006876/ /pubmed/21587932 http://dx.doi.org/10.1107/S1600536810022920 Text en © Li and Jian 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, Yu-Feng
Jian, Fang-Fang
4-Ethyl-1-[4-(methyl­sulfan­yl)benzyl­idene]thio­semicarbazide
title 4-Ethyl-1-[4-(methyl­sulfan­yl)benzyl­idene]thio­semicarbazide
title_full 4-Ethyl-1-[4-(methyl­sulfan­yl)benzyl­idene]thio­semicarbazide
title_fullStr 4-Ethyl-1-[4-(methyl­sulfan­yl)benzyl­idene]thio­semicarbazide
title_full_unstemmed 4-Ethyl-1-[4-(methyl­sulfan­yl)benzyl­idene]thio­semicarbazide
title_short 4-Ethyl-1-[4-(methyl­sulfan­yl)benzyl­idene]thio­semicarbazide
title_sort 4-ethyl-1-[4-(methyl­sulfan­yl)benzyl­idene]thio­semicarbazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3006876/
https://www.ncbi.nlm.nih.gov/pubmed/21587932
http://dx.doi.org/10.1107/S1600536810022920
work_keys_str_mv AT liyufeng 4ethyl14methylsulfanylbenzylidenethiosemicarbazide
AT jianfangfang 4ethyl14methylsulfanylbenzylidenethiosemicarbazide

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