1,3-Bis(4-meth­oxy­benz­yl)-6-methyl­pyrimidine-2,4(1H,3H)-dione

The title compound, C(21)H(22)N(2)O(4), was prepared by reaction of 6-methyl­pyrimidine-2,4(1H,3H)-dione and 1-chloro­methyl-4-meth­oxy­benzene. In the title mol­ecule, the central pyrimidine ring forms dihedral angles of 62.16 (4) and 69.77 (3)° with the two benzene rings. In the crystal, weak inte...

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Detalles Bibliográficos
Autores principales: Li, Gong-Chun, Zhang, Li-Ke, Ju, Zhi-Yu, Yang, Feng-Ling
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3006881/
https://www.ncbi.nlm.nih.gov/pubmed/21588055
http://dx.doi.org/10.1107/S1600536810024815
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author Li, Gong-Chun
Zhang, Li-Ke
Ju, Zhi-Yu
Yang, Feng-Ling
author_facet Li, Gong-Chun
Zhang, Li-Ke
Ju, Zhi-Yu
Yang, Feng-Ling
author_sort Li, Gong-Chun
collection PubMed
description The title compound, C(21)H(22)N(2)O(4), was prepared by reaction of 6-methyl­pyrimidine-2,4(1H,3H)-dione and 1-chloro­methyl-4-meth­oxy­benzene. In the title mol­ecule, the central pyrimidine ring forms dihedral angles of 62.16 (4) and 69.77 (3)° with the two benzene rings. In the crystal, weak inter­molecular C—H⋯O hydrogen bonds link the mol­ecules into chains.
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spelling pubmed-30068812010-12-30 1,3-Bis(4-meth­oxy­benz­yl)-6-methyl­pyrimidine-2,4(1H,3H)-dione Li, Gong-Chun Zhang, Li-Ke Ju, Zhi-Yu Yang, Feng-Ling Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(21)H(22)N(2)O(4), was prepared by reaction of 6-methyl­pyrimidine-2,4(1H,3H)-dione and 1-chloro­methyl-4-meth­oxy­benzene. In the title mol­ecule, the central pyrimidine ring forms dihedral angles of 62.16 (4) and 69.77 (3)° with the two benzene rings. In the crystal, weak inter­molecular C—H⋯O hydrogen bonds link the mol­ecules into chains. International Union of Crystallography 2010-06-30 /pmc/articles/PMC3006881/ /pubmed/21588055 http://dx.doi.org/10.1107/S1600536810024815 Text en © Li et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, Gong-Chun
Zhang, Li-Ke
Ju, Zhi-Yu
Yang, Feng-Ling
1,3-Bis(4-meth­oxy­benz­yl)-6-methyl­pyrimidine-2,4(1H,3H)-dione
title 1,3-Bis(4-meth­oxy­benz­yl)-6-methyl­pyrimidine-2,4(1H,3H)-dione
title_full 1,3-Bis(4-meth­oxy­benz­yl)-6-methyl­pyrimidine-2,4(1H,3H)-dione
title_fullStr 1,3-Bis(4-meth­oxy­benz­yl)-6-methyl­pyrimidine-2,4(1H,3H)-dione
title_full_unstemmed 1,3-Bis(4-meth­oxy­benz­yl)-6-methyl­pyrimidine-2,4(1H,3H)-dione
title_short 1,3-Bis(4-meth­oxy­benz­yl)-6-methyl­pyrimidine-2,4(1H,3H)-dione
title_sort 1,3-bis(4-meth­oxy­benz­yl)-6-methyl­pyrimidine-2,4(1h,3h)-dione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3006881/
https://www.ncbi.nlm.nih.gov/pubmed/21588055
http://dx.doi.org/10.1107/S1600536810024815
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