Ethyl 1,6-dimethyl-2-oxo-4-(quinolin-4-yl)-1,2,3,4-tetra­hydro­pyrimidine-5-carboxyl­ate

In the title compound, C(18)H(19)N(3)O(3), the tetra­hydro­pyrimidone ring adopts a distorted boat conformation. In the crystal structure, inter­molecular N—H⋯O hydrogen bonds link the mol­ecules into centrosymmetric dimers, which are further linked via inter­molecular C—H⋯π inter­actions. In additi...

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Detalles Bibliográficos
Autores principales: Zubatyuk, Roman I., Shishkin, Oleg V., Ihmels, Heiko, Lebedyeva, Iryna A., Povstyanoy, Mykhaylo V.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3006892/
https://www.ncbi.nlm.nih.gov/pubmed/21587977
http://dx.doi.org/10.1107/S1600536810023482
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author Zubatyuk, Roman I.
Shishkin, Oleg V.
Ihmels, Heiko
Lebedyeva, Iryna A.
Povstyanoy, Mykhaylo V.
author_facet Zubatyuk, Roman I.
Shishkin, Oleg V.
Ihmels, Heiko
Lebedyeva, Iryna A.
Povstyanoy, Mykhaylo V.
author_sort Zubatyuk, Roman I.
collection PubMed
description In the title compound, C(18)H(19)N(3)O(3), the tetra­hydro­pyrimidone ring adopts a distorted boat conformation. In the crystal structure, inter­molecular N—H⋯O hydrogen bonds link the mol­ecules into centrosymmetric dimers, which are further linked via inter­molecular C—H⋯π inter­actions. In addition, an intra­molecular C—H⋯O hydrogen bond occurs.
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spelling pubmed-30068922010-12-30 Ethyl 1,6-dimethyl-2-oxo-4-(quinolin-4-yl)-1,2,3,4-tetra­hydro­pyrimidine-5-carboxyl­ate Zubatyuk, Roman I. Shishkin, Oleg V. Ihmels, Heiko Lebedyeva, Iryna A. Povstyanoy, Mykhaylo V. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(18)H(19)N(3)O(3), the tetra­hydro­pyrimidone ring adopts a distorted boat conformation. In the crystal structure, inter­molecular N—H⋯O hydrogen bonds link the mol­ecules into centrosymmetric dimers, which are further linked via inter­molecular C—H⋯π inter­actions. In addition, an intra­molecular C—H⋯O hydrogen bond occurs. International Union of Crystallography 2010-06-23 /pmc/articles/PMC3006892/ /pubmed/21587977 http://dx.doi.org/10.1107/S1600536810023482 Text en © Zubatyuk et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zubatyuk, Roman I.
Shishkin, Oleg V.
Ihmels, Heiko
Lebedyeva, Iryna A.
Povstyanoy, Mykhaylo V.
Ethyl 1,6-dimethyl-2-oxo-4-(quinolin-4-yl)-1,2,3,4-tetra­hydro­pyrimidine-5-carboxyl­ate
title Ethyl 1,6-dimethyl-2-oxo-4-(quinolin-4-yl)-1,2,3,4-tetra­hydro­pyrimidine-5-carboxyl­ate
title_full Ethyl 1,6-dimethyl-2-oxo-4-(quinolin-4-yl)-1,2,3,4-tetra­hydro­pyrimidine-5-carboxyl­ate
title_fullStr Ethyl 1,6-dimethyl-2-oxo-4-(quinolin-4-yl)-1,2,3,4-tetra­hydro­pyrimidine-5-carboxyl­ate
title_full_unstemmed Ethyl 1,6-dimethyl-2-oxo-4-(quinolin-4-yl)-1,2,3,4-tetra­hydro­pyrimidine-5-carboxyl­ate
title_short Ethyl 1,6-dimethyl-2-oxo-4-(quinolin-4-yl)-1,2,3,4-tetra­hydro­pyrimidine-5-carboxyl­ate
title_sort ethyl 1,6-dimethyl-2-oxo-4-(quinolin-4-yl)-1,2,3,4-tetra­hydro­pyrimidine-5-carboxyl­ate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3006892/
https://www.ncbi.nlm.nih.gov/pubmed/21587977
http://dx.doi.org/10.1107/S1600536810023482
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