4-Chloro-N-(3-chloro­benzo­yl)benzene­sulfonamide monohydrate

In the title compound, C(13)H(9)Cl(2)NO(3)S·H(2)O, the conformation of the C=O bond is syn to the meta-Cl group in the benzoyl ring. The mol­ecules are twisted at the S—N bond with a C—S—N—C torsion angle of 72.9 (2)°. The dihedral angle between the sulfonyl benzene ring and the S—NH—C—O segment is...

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Detalles Bibliográficos
Autores principales: Suchetan, P. A., Gowda, B. Thimme, Foro, Sabine, Fuess, Hartmut
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3006969/
https://www.ncbi.nlm.nih.gov/pubmed/21587986
http://dx.doi.org/10.1107/S1600536810023962
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author Suchetan, P. A.
Gowda, B. Thimme
Foro, Sabine
Fuess, Hartmut
author_facet Suchetan, P. A.
Gowda, B. Thimme
Foro, Sabine
Fuess, Hartmut
author_sort Suchetan, P. A.
collection PubMed
description In the title compound, C(13)H(9)Cl(2)NO(3)S·H(2)O, the conformation of the C=O bond is syn to the meta-Cl group in the benzoyl ring. The mol­ecules are twisted at the S—N bond with a C—S—N—C torsion angle of 72.9 (2)°. The dihedral angle between the sulfonyl benzene ring and the S—NH—C—O segment is 77.8 (1)° and that between the sulfonyl and benzoyl benzene rings is 80.5 (1)°. In the crystal, mol­ecules are linked into a two-dimensional network parallel to (100) by N—H⋯O and O—H⋯O hydrogen bonds.
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spelling pubmed-30069692010-12-30 4-Chloro-N-(3-chloro­benzo­yl)benzene­sulfonamide monohydrate Suchetan, P. A. Gowda, B. Thimme Foro, Sabine Fuess, Hartmut Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(13)H(9)Cl(2)NO(3)S·H(2)O, the conformation of the C=O bond is syn to the meta-Cl group in the benzoyl ring. The mol­ecules are twisted at the S—N bond with a C—S—N—C torsion angle of 72.9 (2)°. The dihedral angle between the sulfonyl benzene ring and the S—NH—C—O segment is 77.8 (1)° and that between the sulfonyl and benzoyl benzene rings is 80.5 (1)°. In the crystal, mol­ecules are linked into a two-dimensional network parallel to (100) by N—H⋯O and O—H⋯O hydrogen bonds. International Union of Crystallography 2010-06-26 /pmc/articles/PMC3006969/ /pubmed/21587986 http://dx.doi.org/10.1107/S1600536810023962 Text en © Suchetan et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Suchetan, P. A.
Gowda, B. Thimme
Foro, Sabine
Fuess, Hartmut
4-Chloro-N-(3-chloro­benzo­yl)benzene­sulfonamide monohydrate
title 4-Chloro-N-(3-chloro­benzo­yl)benzene­sulfonamide monohydrate
title_full 4-Chloro-N-(3-chloro­benzo­yl)benzene­sulfonamide monohydrate
title_fullStr 4-Chloro-N-(3-chloro­benzo­yl)benzene­sulfonamide monohydrate
title_full_unstemmed 4-Chloro-N-(3-chloro­benzo­yl)benzene­sulfonamide monohydrate
title_short 4-Chloro-N-(3-chloro­benzo­yl)benzene­sulfonamide monohydrate
title_sort 4-chloro-n-(3-chloro­benzo­yl)benzene­sulfonamide monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3006969/
https://www.ncbi.nlm.nih.gov/pubmed/21587986
http://dx.doi.org/10.1107/S1600536810023962
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AT forosabine 4chloron3chlorobenzoylbenzenesulfonamidemonohydrate
AT fuesshartmut 4chloron3chlorobenzoylbenzenesulfonamidemonohydrate

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