(S)-tert-Butyl 3-(3-phenyl-1,2,4-oxa­diazol-5-yl)piperidine-1-carboxyl­ate

The title compound, C(18)H(23)N(3)O(3), crystallized with two independent mol­ecules (A and B) in the asymmetric unit. The phenyl ring and the 1,2,4-oxadiazole ring are inclined to one another by 19.9 (3)° in mol­ecule A and 7.3 (3)° in mol­ecule B. The absolute structure of the title compound was r...

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Detalles Bibliográficos
Autores principales: Liu, Lin, Xia, Guangxin, Liu, Xuejun, Xie, Jieshu, Shen, Jingkang
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007067/
https://www.ncbi.nlm.nih.gov/pubmed/21587817
http://dx.doi.org/10.1107/S1600536810018714
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author Liu, Lin
Xia, Guangxin
Liu, Xuejun
Xie, Jieshu
Shen, Jingkang
author_facet Liu, Lin
Xia, Guangxin
Liu, Xuejun
Xie, Jieshu
Shen, Jingkang
author_sort Liu, Lin
collection PubMed
description The title compound, C(18)H(23)N(3)O(3), crystallized with two independent mol­ecules (A and B) in the asymmetric unit. The phenyl ring and the 1,2,4-oxadiazole ring are inclined to one another by 19.9 (3)° in mol­ecule A and 7.3 (3)° in mol­ecule B. The absolute structure of the title compound was referred to the transfered chiral center (S) of one of the starting reacta­nts. In the crystal, A mol­ecules are linked by C—H⋯N inter­actions involving the two oxadiazole N atoms.
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spelling pubmed-30070672010-12-30 (S)-tert-Butyl 3-(3-phenyl-1,2,4-oxa­diazol-5-yl)piperidine-1-carboxyl­ate Liu, Lin Xia, Guangxin Liu, Xuejun Xie, Jieshu Shen, Jingkang Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(18)H(23)N(3)O(3), crystallized with two independent mol­ecules (A and B) in the asymmetric unit. The phenyl ring and the 1,2,4-oxadiazole ring are inclined to one another by 19.9 (3)° in mol­ecule A and 7.3 (3)° in mol­ecule B. The absolute structure of the title compound was referred to the transfered chiral center (S) of one of the starting reacta­nts. In the crystal, A mol­ecules are linked by C—H⋯N inter­actions involving the two oxadiazole N atoms. International Union of Crystallography 2010-06-05 /pmc/articles/PMC3007067/ /pubmed/21587817 http://dx.doi.org/10.1107/S1600536810018714 Text en © Liu et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Liu, Lin
Xia, Guangxin
Liu, Xuejun
Xie, Jieshu
Shen, Jingkang
(S)-tert-Butyl 3-(3-phenyl-1,2,4-oxa­diazol-5-yl)piperidine-1-carboxyl­ate
title (S)-tert-Butyl 3-(3-phenyl-1,2,4-oxa­diazol-5-yl)piperidine-1-carboxyl­ate
title_full (S)-tert-Butyl 3-(3-phenyl-1,2,4-oxa­diazol-5-yl)piperidine-1-carboxyl­ate
title_fullStr (S)-tert-Butyl 3-(3-phenyl-1,2,4-oxa­diazol-5-yl)piperidine-1-carboxyl­ate
title_full_unstemmed (S)-tert-Butyl 3-(3-phenyl-1,2,4-oxa­diazol-5-yl)piperidine-1-carboxyl­ate
title_short (S)-tert-Butyl 3-(3-phenyl-1,2,4-oxa­diazol-5-yl)piperidine-1-carboxyl­ate
title_sort (s)-tert-butyl 3-(3-phenyl-1,2,4-oxa­diazol-5-yl)piperidine-1-carboxyl­ate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007067/
https://www.ncbi.nlm.nih.gov/pubmed/21587817
http://dx.doi.org/10.1107/S1600536810018714
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AT liuxuejun stertbutyl33phenyl124oxadiazol5ylpiperidine1carboxylate
AT xiejieshu stertbutyl33phenyl124oxadiazol5ylpiperidine1carboxylate
AT shenjingkang stertbutyl33phenyl124oxadiazol5ylpiperidine1carboxylate

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