(4-Chloro­phen­yl)(3,6-dibromo-2-hy­droxy-7-meth­oxy-1-naphth­yl)methanone

The asymmetric unit of the title compound, C(18)H(11)Br(2)ClO(3), contains two crystallographically independent mol­ecules in which the dihedral angles between the naphthalene ring systems and the benzene rings are 55.64 (11) and 60.50 (11)°. In each mol­ecule, an intra­molecular O—H⋯O=C hydrogen bo...

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Autores principales: Mitsui, Ryosuke, Nagasawa, Atsushi, Watanabe, Shoji, Okamoto, Akiko, Yonezawa, Noriyuki
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007072/
https://www.ncbi.nlm.nih.gov/pubmed/21587976
http://dx.doi.org/10.1107/S1600536810023299
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author Mitsui, Ryosuke
Nagasawa, Atsushi
Watanabe, Shoji
Okamoto, Akiko
Yonezawa, Noriyuki
author_facet Mitsui, Ryosuke
Nagasawa, Atsushi
Watanabe, Shoji
Okamoto, Akiko
Yonezawa, Noriyuki
author_sort Mitsui, Ryosuke
collection PubMed
description The asymmetric unit of the title compound, C(18)H(11)Br(2)ClO(3), contains two crystallographically independent mol­ecules in which the dihedral angles between the naphthalene ring systems and the benzene rings are 55.64 (11) and 60.50 (11)°. In each mol­ecule, an intra­molecular O—H⋯O=C hydrogen bond generates a six-membered ring. In the crystal structure, inter­molecular C—H⋯O and C—H⋯Cl hydrogen bonds and two different Br⋯O halogen bonds [2.9850 (19) and 3.2169 (19) Å] are observed.
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spelling pubmed-30070722010-12-30 (4-Chloro­phen­yl)(3,6-dibromo-2-hy­droxy-7-meth­oxy-1-naphth­yl)methanone Mitsui, Ryosuke Nagasawa, Atsushi Watanabe, Shoji Okamoto, Akiko Yonezawa, Noriyuki Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(18)H(11)Br(2)ClO(3), contains two crystallographically independent mol­ecules in which the dihedral angles between the naphthalene ring systems and the benzene rings are 55.64 (11) and 60.50 (11)°. In each mol­ecule, an intra­molecular O—H⋯O=C hydrogen bond generates a six-membered ring. In the crystal structure, inter­molecular C—H⋯O and C—H⋯Cl hydrogen bonds and two different Br⋯O halogen bonds [2.9850 (19) and 3.2169 (19) Å] are observed. International Union of Crystallography 2010-06-23 /pmc/articles/PMC3007072/ /pubmed/21587976 http://dx.doi.org/10.1107/S1600536810023299 Text en © Mitsui et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Mitsui, Ryosuke
Nagasawa, Atsushi
Watanabe, Shoji
Okamoto, Akiko
Yonezawa, Noriyuki
(4-Chloro­phen­yl)(3,6-dibromo-2-hy­droxy-7-meth­oxy-1-naphth­yl)methanone
title (4-Chloro­phen­yl)(3,6-dibromo-2-hy­droxy-7-meth­oxy-1-naphth­yl)methanone
title_full (4-Chloro­phen­yl)(3,6-dibromo-2-hy­droxy-7-meth­oxy-1-naphth­yl)methanone
title_fullStr (4-Chloro­phen­yl)(3,6-dibromo-2-hy­droxy-7-meth­oxy-1-naphth­yl)methanone
title_full_unstemmed (4-Chloro­phen­yl)(3,6-dibromo-2-hy­droxy-7-meth­oxy-1-naphth­yl)methanone
title_short (4-Chloro­phen­yl)(3,6-dibromo-2-hy­droxy-7-meth­oxy-1-naphth­yl)methanone
title_sort (4-chloro­phen­yl)(3,6-dibromo-2-hy­droxy-7-meth­oxy-1-naphth­yl)methanone
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007072/
https://www.ncbi.nlm.nih.gov/pubmed/21587976
http://dx.doi.org/10.1107/S1600536810023299
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