6,7,8,9-Tetra­hydro-4b,9b-dihy­droxy­indano[1,2-b]indoline-9,10-dione monohydrate

In the title compound, C(15)H(13)NO(4)·H(2)O, the organic mol­ecule adopts a V-shaped conformation in which the dihedral angle between the five-membered rings is 68.33 (5)°. The cyclo­hexenone ring adopts an envelope conformation, with one of the methyl­ene C atoms displaced by 0.607 (4) Å from the...

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Detalles Bibliográficos
Autores principales: Yaqub, Muhammad, Mahmood, Khalid, Tahir, M. Nawaz, Shafiq, Zahid, Rauf, Abdul
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007351/
https://www.ncbi.nlm.nih.gov/pubmed/21588222
http://dx.doi.org/10.1107/S1600536810025328
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author Yaqub, Muhammad
Mahmood, Khalid
Tahir, M. Nawaz
Shafiq, Zahid
Rauf, Abdul
author_facet Yaqub, Muhammad
Mahmood, Khalid
Tahir, M. Nawaz
Shafiq, Zahid
Rauf, Abdul
author_sort Yaqub, Muhammad
collection PubMed
description In the title compound, C(15)H(13)NO(4)·H(2)O, the organic mol­ecule adopts a V-shaped conformation in which the dihedral angle between the five-membered rings is 68.33 (5)°. The cyclo­hexenone ring adopts an envelope conformation, with one of the methyl­ene C atoms displaced by 0.607 (4) Å from the plane through the other atoms. In the crystal, inter­molecular N—H⋯(O,O) and O—H⋯O hydrogen bonds link the components into (001) sheeets and C–H⋯O inter­actions and aromatic π–π stacking [centroid–centroid separation = 3.6176 (19) Å] help to consolidate the packing.
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spelling pubmed-30073512010-12-30 6,7,8,9-Tetra­hydro-4b,9b-dihy­droxy­indano[1,2-b]indoline-9,10-dione monohydrate Yaqub, Muhammad Mahmood, Khalid Tahir, M. Nawaz Shafiq, Zahid Rauf, Abdul Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(15)H(13)NO(4)·H(2)O, the organic mol­ecule adopts a V-shaped conformation in which the dihedral angle between the five-membered rings is 68.33 (5)°. The cyclo­hexenone ring adopts an envelope conformation, with one of the methyl­ene C atoms displaced by 0.607 (4) Å from the plane through the other atoms. In the crystal, inter­molecular N—H⋯(O,O) and O—H⋯O hydrogen bonds link the components into (001) sheeets and C–H⋯O inter­actions and aromatic π–π stacking [centroid–centroid separation = 3.6176 (19) Å] help to consolidate the packing. International Union of Crystallography 2010-07-03 /pmc/articles/PMC3007351/ /pubmed/21588222 http://dx.doi.org/10.1107/S1600536810025328 Text en © Yaqub et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Yaqub, Muhammad
Mahmood, Khalid
Tahir, M. Nawaz
Shafiq, Zahid
Rauf, Abdul
6,7,8,9-Tetra­hydro-4b,9b-dihy­droxy­indano[1,2-b]indoline-9,10-dione monohydrate
title 6,7,8,9-Tetra­hydro-4b,9b-dihy­droxy­indano[1,2-b]indoline-9,10-dione monohydrate
title_full 6,7,8,9-Tetra­hydro-4b,9b-dihy­droxy­indano[1,2-b]indoline-9,10-dione monohydrate
title_fullStr 6,7,8,9-Tetra­hydro-4b,9b-dihy­droxy­indano[1,2-b]indoline-9,10-dione monohydrate
title_full_unstemmed 6,7,8,9-Tetra­hydro-4b,9b-dihy­droxy­indano[1,2-b]indoline-9,10-dione monohydrate
title_short 6,7,8,9-Tetra­hydro-4b,9b-dihy­droxy­indano[1,2-b]indoline-9,10-dione monohydrate
title_sort 6,7,8,9-tetra­hydro-4b,9b-dihy­droxy­indano[1,2-b]indoline-9,10-dione monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007351/
https://www.ncbi.nlm.nih.gov/pubmed/21588222
http://dx.doi.org/10.1107/S1600536810025328
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