2-Amino-5-bromo­pyridine–4-hy­droxy­benzoic acid (1/1)

The title 1:1 adduct, C(5)H(5)BrN(2)·C(7)H(6)O(3), contains two mol­ecules of each species in the asymmetric unit, with similar geometries. In the crystal, mol­ecules are linked to form extended chains along [100] by N—H⋯O, O—H⋯O, O—H⋯N and C—H⋯O hydrogen bonds. Adjacent chains are crosslinked via f...

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Detalles Bibliográficos
Autores principales: Quah, Ching Kheng, Hemamalini, Madhukar, Fun, Hoong-Kun
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007384/
https://www.ncbi.nlm.nih.gov/pubmed/21588263
http://dx.doi.org/10.1107/S1600536810025924
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author Quah, Ching Kheng
Hemamalini, Madhukar
Fun, Hoong-Kun
author_facet Quah, Ching Kheng
Hemamalini, Madhukar
Fun, Hoong-Kun
author_sort Quah, Ching Kheng
collection PubMed
description The title 1:1 adduct, C(5)H(5)BrN(2)·C(7)H(6)O(3), contains two mol­ecules of each species in the asymmetric unit, with similar geometries. In the crystal, mol­ecules are linked to form extended chains along [100] by N—H⋯O, O—H⋯O, O—H⋯N and C—H⋯O hydrogen bonds. Adjacent chains are crosslinked via further N—H⋯O inter­actions into sheets lying parallel to (001). The crystal studied was an inversion twin with a 0.54 (2):0.46 (2) domain ratio.
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spelling pubmed-30073842010-12-30 2-Amino-5-bromo­pyridine–4-hy­droxy­benzoic acid (1/1) Quah, Ching Kheng Hemamalini, Madhukar Fun, Hoong-Kun Acta Crystallogr Sect E Struct Rep Online Organic Papers The title 1:1 adduct, C(5)H(5)BrN(2)·C(7)H(6)O(3), contains two mol­ecules of each species in the asymmetric unit, with similar geometries. In the crystal, mol­ecules are linked to form extended chains along [100] by N—H⋯O, O—H⋯O, O—H⋯N and C—H⋯O hydrogen bonds. Adjacent chains are crosslinked via further N—H⋯O inter­actions into sheets lying parallel to (001). The crystal studied was an inversion twin with a 0.54 (2):0.46 (2) domain ratio. International Union of Crystallography 2010-07-07 /pmc/articles/PMC3007384/ /pubmed/21588263 http://dx.doi.org/10.1107/S1600536810025924 Text en © Quah et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Quah, Ching Kheng
Hemamalini, Madhukar
Fun, Hoong-Kun
2-Amino-5-bromo­pyridine–4-hy­droxy­benzoic acid (1/1)
title 2-Amino-5-bromo­pyridine–4-hy­droxy­benzoic acid (1/1)
title_full 2-Amino-5-bromo­pyridine–4-hy­droxy­benzoic acid (1/1)
title_fullStr 2-Amino-5-bromo­pyridine–4-hy­droxy­benzoic acid (1/1)
title_full_unstemmed 2-Amino-5-bromo­pyridine–4-hy­droxy­benzoic acid (1/1)
title_short 2-Amino-5-bromo­pyridine–4-hy­droxy­benzoic acid (1/1)
title_sort 2-amino-5-bromo­pyridine–4-hy­droxy­benzoic acid (1/1)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007384/
https://www.ncbi.nlm.nih.gov/pubmed/21588263
http://dx.doi.org/10.1107/S1600536810025924
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AT hemamalinimadhukar 2amino5bromopyridine4hydroxybenzoicacid11
AT funhoongkun 2amino5bromopyridine4hydroxybenzoicacid11

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