2-[1-(3-Oxo-1,3-dihydro-2-benzofuran-1-yl)-1H-benzimidazol-2-yl]benzoic acid methanol solvate

The condensation of 2-carb­oxy­benzaldehyde with 1,2-phenyl­enediamine unexpectedly yielded the title compound, C(22)H(14)N(2)O(4)·CH(4)O. The benzimidazole ring system is almost perpendicular to the phthalazine ring system, making a dihedral angle of 88.4 (5)°. Inter­molecular O—H⋯N and O—H⋯O hydro...

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Detalles Bibliográficos
Autores principales: Shi, Guang, Ma, Li, Deng, Hong
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007451/
https://www.ncbi.nlm.nih.gov/pubmed/21588343
http://dx.doi.org/10.1107/S1600536810026851
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author Shi, Guang
Ma, Li
Deng, Hong
author_facet Shi, Guang
Ma, Li
Deng, Hong
author_sort Shi, Guang
collection PubMed
description The condensation of 2-carb­oxy­benzaldehyde with 1,2-phenyl­enediamine unexpectedly yielded the title compound, C(22)H(14)N(2)O(4)·CH(4)O. The benzimidazole ring system is almost perpendicular to the phthalazine ring system, making a dihedral angle of 88.4 (5)°. Inter­molecular O—H⋯N and O—H⋯O hydrogen-bonding inter­actions stabilize the crystal structure.
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spelling pubmed-30074512010-12-30 2-[1-(3-Oxo-1,3-dihydro-2-benzofuran-1-yl)-1H-benzimidazol-2-yl]benzoic acid methanol solvate Shi, Guang Ma, Li Deng, Hong Acta Crystallogr Sect E Struct Rep Online Organic Papers The condensation of 2-carb­oxy­benzaldehyde with 1,2-phenyl­enediamine unexpectedly yielded the title compound, C(22)H(14)N(2)O(4)·CH(4)O. The benzimidazole ring system is almost perpendicular to the phthalazine ring system, making a dihedral angle of 88.4 (5)°. Inter­molecular O—H⋯N and O—H⋯O hydrogen-bonding inter­actions stabilize the crystal structure. International Union of Crystallography 2010-07-17 /pmc/articles/PMC3007451/ /pubmed/21588343 http://dx.doi.org/10.1107/S1600536810026851 Text en © Shi et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Shi, Guang
Ma, Li
Deng, Hong
2-[1-(3-Oxo-1,3-dihydro-2-benzofuran-1-yl)-1H-benzimidazol-2-yl]benzoic acid methanol solvate
title 2-[1-(3-Oxo-1,3-dihydro-2-benzofuran-1-yl)-1H-benzimidazol-2-yl]benzoic acid methanol solvate
title_full 2-[1-(3-Oxo-1,3-dihydro-2-benzofuran-1-yl)-1H-benzimidazol-2-yl]benzoic acid methanol solvate
title_fullStr 2-[1-(3-Oxo-1,3-dihydro-2-benzofuran-1-yl)-1H-benzimidazol-2-yl]benzoic acid methanol solvate
title_full_unstemmed 2-[1-(3-Oxo-1,3-dihydro-2-benzofuran-1-yl)-1H-benzimidazol-2-yl]benzoic acid methanol solvate
title_short 2-[1-(3-Oxo-1,3-dihydro-2-benzofuran-1-yl)-1H-benzimidazol-2-yl]benzoic acid methanol solvate
title_sort 2-[1-(3-oxo-1,3-dihydro-2-benzofuran-1-yl)-1h-benzimidazol-2-yl]benzoic acid methanol solvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007451/
https://www.ncbi.nlm.nih.gov/pubmed/21588343
http://dx.doi.org/10.1107/S1600536810026851
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AT denghong 213oxo13dihydro2benzofuran1yl1hbenzimidazol2ylbenzoicacidmethanolsolvate

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