2-[2-(2-Anilino-4-oxo-3,4-dihydro­quinazolin-3-yl)phen­oxy]-3-phenyl­quinazolin-4(3H)-one methanol hemisolvate

In the title compound, C(34)H(23)N(5)O(3)·0.5CH(3)OH, each pyrimid­in­one heterocycle and its adjacent benzene ring are almost coplanar, making dihedral angles of 0.69 (13) and 1.87 (13)°. The lower pyrimidinone ring makes a dihedral angle of 40.41 (15)° with the —NH— bonded phenyl ring. O—H⋯O hydro...

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Detalles Bibliográficos
Autores principales: Gao, Tao, Chen, Xiao-Bao, Yang, Xu-Hong, Wang, Xiang
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007481/
https://www.ncbi.nlm.nih.gov/pubmed/21588376
http://dx.doi.org/10.1107/S1600536810028011
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author Gao, Tao
Chen, Xiao-Bao
Yang, Xu-Hong
Wang, Xiang
author_facet Gao, Tao
Chen, Xiao-Bao
Yang, Xu-Hong
Wang, Xiang
author_sort Gao, Tao
collection PubMed
description In the title compound, C(34)H(23)N(5)O(3)·0.5CH(3)OH, each pyrimid­in­one heterocycle and its adjacent benzene ring are almost coplanar, making dihedral angles of 0.69 (13) and 1.87 (13)°. The lower pyrimidinone ring makes a dihedral angle of 40.41 (15)° with the —NH— bonded phenyl ring. O—H⋯O hydrogen bonds and weak C—H⋯π inter­actions are observed in the crystal structure. The methanol solvent molecule is disordered over two positions of equal occupancy.
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spelling pubmed-30074812010-12-30 2-[2-(2-Anilino-4-oxo-3,4-dihydro­quinazolin-3-yl)phen­oxy]-3-phenyl­quinazolin-4(3H)-one methanol hemisolvate Gao, Tao Chen, Xiao-Bao Yang, Xu-Hong Wang, Xiang Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(34)H(23)N(5)O(3)·0.5CH(3)OH, each pyrimid­in­one heterocycle and its adjacent benzene ring are almost coplanar, making dihedral angles of 0.69 (13) and 1.87 (13)°. The lower pyrimidinone ring makes a dihedral angle of 40.41 (15)° with the —NH— bonded phenyl ring. O—H⋯O hydrogen bonds and weak C—H⋯π inter­actions are observed in the crystal structure. The methanol solvent molecule is disordered over two positions of equal occupancy. International Union of Crystallography 2010-07-21 /pmc/articles/PMC3007481/ /pubmed/21588376 http://dx.doi.org/10.1107/S1600536810028011 Text en © Gao et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Gao, Tao
Chen, Xiao-Bao
Yang, Xu-Hong
Wang, Xiang
2-[2-(2-Anilino-4-oxo-3,4-dihydro­quinazolin-3-yl)phen­oxy]-3-phenyl­quinazolin-4(3H)-one methanol hemisolvate
title 2-[2-(2-Anilino-4-oxo-3,4-dihydro­quinazolin-3-yl)phen­oxy]-3-phenyl­quinazolin-4(3H)-one methanol hemisolvate
title_full 2-[2-(2-Anilino-4-oxo-3,4-dihydro­quinazolin-3-yl)phen­oxy]-3-phenyl­quinazolin-4(3H)-one methanol hemisolvate
title_fullStr 2-[2-(2-Anilino-4-oxo-3,4-dihydro­quinazolin-3-yl)phen­oxy]-3-phenyl­quinazolin-4(3H)-one methanol hemisolvate
title_full_unstemmed 2-[2-(2-Anilino-4-oxo-3,4-dihydro­quinazolin-3-yl)phen­oxy]-3-phenyl­quinazolin-4(3H)-one methanol hemisolvate
title_short 2-[2-(2-Anilino-4-oxo-3,4-dihydro­quinazolin-3-yl)phen­oxy]-3-phenyl­quinazolin-4(3H)-one methanol hemisolvate
title_sort 2-[2-(2-anilino-4-oxo-3,4-dihydro­quinazolin-3-yl)phen­oxy]-3-phenyl­quinazolin-4(3h)-one methanol hemisolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007481/
https://www.ncbi.nlm.nih.gov/pubmed/21588376
http://dx.doi.org/10.1107/S1600536810028011
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