Methyl 4-isonicotinamido­benzoate monohydrate

The title compound, C(14)H(12)N(2)O(3)·H(2)O, synthesized by the reaction of methyl 4-amino­benzoate with isonicotinoyl chloride hydro­chloride, is relatively planar, with the pyridine ring being inclined by 7.46 (7)° to the benzene ring. In the crystal, the methyl 4-isonicotinamido­benzoate mol­ecu...

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Detalles Bibliográficos
Autores principales: Zhang, Yang, Zhao, Xiao-Li
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007520/
https://www.ncbi.nlm.nih.gov/pubmed/21588232
http://dx.doi.org/10.1107/S1600536810024979
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author Zhang, Yang
Zhao, Xiao-Li
author_facet Zhang, Yang
Zhao, Xiao-Li
author_sort Zhang, Yang
collection PubMed
description The title compound, C(14)H(12)N(2)O(3)·H(2)O, synthesized by the reaction of methyl 4-amino­benzoate with isonicotinoyl chloride hydro­chloride, is relatively planar, with the pyridine ring being inclined by 7.46 (7)° to the benzene ring. In the crystal, the methyl 4-isonicotinamido­benzoate mol­ecules are inter­linked by water mol­ecules via N—H⋯O, O—H⋯N and O—H⋯O hydrogen bonds, leading to the formation of a double-chain ribbon-like structure.
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spelling pubmed-30075202010-12-30 Methyl 4-isonicotinamido­benzoate monohydrate Zhang, Yang Zhao, Xiao-Li Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(14)H(12)N(2)O(3)·H(2)O, synthesized by the reaction of methyl 4-amino­benzoate with isonicotinoyl chloride hydro­chloride, is relatively planar, with the pyridine ring being inclined by 7.46 (7)° to the benzene ring. In the crystal, the methyl 4-isonicotinamido­benzoate mol­ecules are inter­linked by water mol­ecules via N—H⋯O, O—H⋯N and O—H⋯O hydrogen bonds, leading to the formation of a double-chain ribbon-like structure. International Union of Crystallography 2010-07-03 /pmc/articles/PMC3007520/ /pubmed/21588232 http://dx.doi.org/10.1107/S1600536810024979 Text en © Zhang and Zhao 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhang, Yang
Zhao, Xiao-Li
Methyl 4-isonicotinamido­benzoate monohydrate
title Methyl 4-isonicotinamido­benzoate monohydrate
title_full Methyl 4-isonicotinamido­benzoate monohydrate
title_fullStr Methyl 4-isonicotinamido­benzoate monohydrate
title_full_unstemmed Methyl 4-isonicotinamido­benzoate monohydrate
title_short Methyl 4-isonicotinamido­benzoate monohydrate
title_sort methyl 4-isonicotinamido­benzoate monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007520/
https://www.ncbi.nlm.nih.gov/pubmed/21588232
http://dx.doi.org/10.1107/S1600536810024979
work_keys_str_mv AT zhangyang methyl4isonicotinamidobenzoatemonohydrate
AT zhaoxiaoli methyl4isonicotinamidobenzoatemonohydrate

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