5-(3,4,5-Trimeth­oxy­phen­yl)-1,3,4-oxadiazole-2(3H)-thione

The two rings in the title compound, C(11)H(12)N(2)O(4)S, are roughly coplanar [dihedral angle = 6.77 (8)°]. Whereas the two outer methyl groups of the three meth­oxy groups are almost coplanar with the aromatic ring to which they are attached [C—C—O—C torsion angles = 8.5 (3) and −8.3 (3)°], the me...

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Detalles Bibliográficos
Autores principales: Saeed, Aamer, Akram, Muhammad, Rauf, Abdul, Bolte, Michael
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007562/
https://www.ncbi.nlm.nih.gov/pubmed/21588243
http://dx.doi.org/10.1107/S1600536810024967
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author Saeed, Aamer
Akram, Muhammad
Rauf, Abdul
Bolte, Michael
author_facet Saeed, Aamer
Akram, Muhammad
Rauf, Abdul
Bolte, Michael
author_sort Saeed, Aamer
collection PubMed
description The two rings in the title compound, C(11)H(12)N(2)O(4)S, are roughly coplanar [dihedral angle = 6.77 (8)°]. Whereas the two outer methyl groups of the three meth­oxy groups are almost coplanar with the aromatic ring to which they are attached [C—C—O—C torsion angles = 8.5 (3) and −8.3 (3)°], the methyl group of the central meth­oxy substituent is not [C—C—C—C = −78.4 (3)°]. The crystal packing is stabilized by N—H⋯O hydrogen bonding.
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spelling pubmed-30075622010-12-30 5-(3,4,5-Trimeth­oxy­phen­yl)-1,3,4-oxadiazole-2(3H)-thione Saeed, Aamer Akram, Muhammad Rauf, Abdul Bolte, Michael Acta Crystallogr Sect E Struct Rep Online Organic Papers The two rings in the title compound, C(11)H(12)N(2)O(4)S, are roughly coplanar [dihedral angle = 6.77 (8)°]. Whereas the two outer methyl groups of the three meth­oxy groups are almost coplanar with the aromatic ring to which they are attached [C—C—O—C torsion angles = 8.5 (3) and −8.3 (3)°], the methyl group of the central meth­oxy substituent is not [C—C—C—C = −78.4 (3)°]. The crystal packing is stabilized by N—H⋯O hydrogen bonding. International Union of Crystallography 2010-07-03 /pmc/articles/PMC3007562/ /pubmed/21588243 http://dx.doi.org/10.1107/S1600536810024967 Text en © Saeed et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Saeed, Aamer
Akram, Muhammad
Rauf, Abdul
Bolte, Michael
5-(3,4,5-Trimeth­oxy­phen­yl)-1,3,4-oxadiazole-2(3H)-thione
title 5-(3,4,5-Trimeth­oxy­phen­yl)-1,3,4-oxadiazole-2(3H)-thione
title_full 5-(3,4,5-Trimeth­oxy­phen­yl)-1,3,4-oxadiazole-2(3H)-thione
title_fullStr 5-(3,4,5-Trimeth­oxy­phen­yl)-1,3,4-oxadiazole-2(3H)-thione
title_full_unstemmed 5-(3,4,5-Trimeth­oxy­phen­yl)-1,3,4-oxadiazole-2(3H)-thione
title_short 5-(3,4,5-Trimeth­oxy­phen­yl)-1,3,4-oxadiazole-2(3H)-thione
title_sort 5-(3,4,5-trimeth­oxy­phen­yl)-1,3,4-oxadiazole-2(3h)-thione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007562/
https://www.ncbi.nlm.nih.gov/pubmed/21588243
http://dx.doi.org/10.1107/S1600536810024967
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AT boltemichael 5345trimethoxyphenyl134oxadiazole23hthione

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