Cargando…
Diethyl 2-[(3,5-dimethyl-1H-pyrazol-1-yl)(4-methoxyphenyl)methyl]propanedioate
The title compound, C(20)H(26)N(2)O(5), was prepared in good yield (76%) through condensation of diethyl (4-methoxybenzyl)propanedioate with 3,5-dimethyl-1H-pyrazole. The dihedral between the benzene and pyrazole rings is 83.96 (10)°. The crystal packing is stabilized by a C—H⋯O interaction, wh...
Autores principales: | , , , , |
---|---|
Formato: | Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2010
|
Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007575/ https://www.ncbi.nlm.nih.gov/pubmed/21588286 http://dx.doi.org/10.1107/S1600536810025572 |
_version_ | 1782194390660284416 |
---|---|
author | Meskini, Ihssan Daoudi, Maria Daran, Jean-Claude Kerbal, Abdelali Zouihri, Hafid |
author_facet | Meskini, Ihssan Daoudi, Maria Daran, Jean-Claude Kerbal, Abdelali Zouihri, Hafid |
author_sort | Meskini, Ihssan |
collection | PubMed |
description | The title compound, C(20)H(26)N(2)O(5), was prepared in good yield (76%) through condensation of diethyl (4-methoxybenzyl)propanedioate with 3,5-dimethyl-1H-pyrazole. The dihedral between the benzene and pyrazole rings is 83.96 (10)°. The crystal packing is stabilized by a C—H⋯O interaction, which links the molecules into centrosymmetric dimers. |
format | Text |
id | pubmed-3007575 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2010 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-30075752010-12-30 Diethyl 2-[(3,5-dimethyl-1H-pyrazol-1-yl)(4-methoxyphenyl)methyl]propanedioate Meskini, Ihssan Daoudi, Maria Daran, Jean-Claude Kerbal, Abdelali Zouihri, Hafid Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(20)H(26)N(2)O(5), was prepared in good yield (76%) through condensation of diethyl (4-methoxybenzyl)propanedioate with 3,5-dimethyl-1H-pyrazole. The dihedral between the benzene and pyrazole rings is 83.96 (10)°. The crystal packing is stabilized by a C—H⋯O interaction, which links the molecules into centrosymmetric dimers. International Union of Crystallography 2010-07-10 /pmc/articles/PMC3007575/ /pubmed/21588286 http://dx.doi.org/10.1107/S1600536810025572 Text en © Meskini et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Meskini, Ihssan Daoudi, Maria Daran, Jean-Claude Kerbal, Abdelali Zouihri, Hafid Diethyl 2-[(3,5-dimethyl-1H-pyrazol-1-yl)(4-methoxyphenyl)methyl]propanedioate |
title | Diethyl 2-[(3,5-dimethyl-1H-pyrazol-1-yl)(4-methoxyphenyl)methyl]propanedioate |
title_full | Diethyl 2-[(3,5-dimethyl-1H-pyrazol-1-yl)(4-methoxyphenyl)methyl]propanedioate |
title_fullStr | Diethyl 2-[(3,5-dimethyl-1H-pyrazol-1-yl)(4-methoxyphenyl)methyl]propanedioate |
title_full_unstemmed | Diethyl 2-[(3,5-dimethyl-1H-pyrazol-1-yl)(4-methoxyphenyl)methyl]propanedioate |
title_short | Diethyl 2-[(3,5-dimethyl-1H-pyrazol-1-yl)(4-methoxyphenyl)methyl]propanedioate |
title_sort | diethyl 2-[(3,5-dimethyl-1h-pyrazol-1-yl)(4-methoxyphenyl)methyl]propanedioate |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007575/ https://www.ncbi.nlm.nih.gov/pubmed/21588286 http://dx.doi.org/10.1107/S1600536810025572 |
work_keys_str_mv | AT meskiniihssan diethyl235dimethyl1hpyrazol1yl4methoxyphenylmethylpropanedioate AT daoudimaria diethyl235dimethyl1hpyrazol1yl4methoxyphenylmethylpropanedioate AT daranjeanclaude diethyl235dimethyl1hpyrazol1yl4methoxyphenylmethylpropanedioate AT kerbalabdelali diethyl235dimethyl1hpyrazol1yl4methoxyphenylmethylpropanedioate AT zouihrihafid diethyl235dimethyl1hpyrazol1yl4methoxyphenylmethylpropanedioate |