3-Eth­oxy-2-hy­droxy­benzaldehyde 2,4-di­nitro­phenylhydrazone N,N-di­methyl­formamide monosolvate

The Schiff base of the title compound, C(15)H(14)N(4)O(6)·C(3)H(7)NO, was obtained from the condensation reaction of 3-eth­oxy-2-hy­droxy­benzaldehyde and 2,4-dinitro­phenyl­hydrazine. The dihedral angle between the benzene rings is 3.05 (10)° and intra­molecular N—H⋯O and O—H⋯O hydrogen bonds gener...

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Detalles Bibliográficos
Autores principales: Zhao, Lin-xiu, Cui, Jian-lan, Cao, Duan-lin
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007826/
https://www.ncbi.nlm.nih.gov/pubmed/21588577
http://dx.doi.org/10.1107/S1600536810029983
Descripción
Sumario:The Schiff base of the title compound, C(15)H(14)N(4)O(6)·C(3)H(7)NO, was obtained from the condensation reaction of 3-eth­oxy-2-hy­droxy­benzaldehyde and 2,4-dinitro­phenyl­hydrazine. The dihedral angle between the benzene rings is 3.05 (10)° and intra­molecular N—H⋯O and O—H⋯O hydrogen bonds generate S(6) and S(5) ring motifs, respectively. In the crystal, the Schiff base and dimethyl­formamide solvent mol­ecules are linked by an O—H⋯O hydrogen bond.

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