3-Eth­oxy-2-hy­droxy­benzaldehyde 2,4-di­nitro­phenylhydrazone N,N-di­methyl­formamide monosolvate

The Schiff base of the title compound, C(15)H(14)N(4)O(6)·C(3)H(7)NO, was obtained from the condensation reaction of 3-eth­oxy-2-hy­droxy­benzaldehyde and 2,4-dinitro­phenyl­hydrazine. The dihedral angle between the benzene rings is 3.05 (10)° and intra­molecular N—H⋯O and O—H⋯O hydrogen bonds gener...

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Detalles Bibliográficos
Autores principales: Zhao, Lin-xiu, Cui, Jian-lan, Cao, Duan-lin
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007826/
https://www.ncbi.nlm.nih.gov/pubmed/21588577
http://dx.doi.org/10.1107/S1600536810029983
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author Zhao, Lin-xiu
Cui, Jian-lan
Cao, Duan-lin
author_facet Zhao, Lin-xiu
Cui, Jian-lan
Cao, Duan-lin
author_sort Zhao, Lin-xiu
collection PubMed
description The Schiff base of the title compound, C(15)H(14)N(4)O(6)·C(3)H(7)NO, was obtained from the condensation reaction of 3-eth­oxy-2-hy­droxy­benzaldehyde and 2,4-dinitro­phenyl­hydrazine. The dihedral angle between the benzene rings is 3.05 (10)° and intra­molecular N—H⋯O and O—H⋯O hydrogen bonds generate S(6) and S(5) ring motifs, respectively. In the crystal, the Schiff base and dimethyl­formamide solvent mol­ecules are linked by an O—H⋯O hydrogen bond.
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spelling pubmed-30078262010-12-30 3-Eth­oxy-2-hy­droxy­benzaldehyde 2,4-di­nitro­phenylhydrazone N,N-di­methyl­formamide monosolvate Zhao, Lin-xiu Cui, Jian-lan Cao, Duan-lin Acta Crystallogr Sect E Struct Rep Online Organic Papers The Schiff base of the title compound, C(15)H(14)N(4)O(6)·C(3)H(7)NO, was obtained from the condensation reaction of 3-eth­oxy-2-hy­droxy­benzaldehyde and 2,4-dinitro­phenyl­hydrazine. The dihedral angle between the benzene rings is 3.05 (10)° and intra­molecular N—H⋯O and O—H⋯O hydrogen bonds generate S(6) and S(5) ring motifs, respectively. In the crystal, the Schiff base and dimethyl­formamide solvent mol­ecules are linked by an O—H⋯O hydrogen bond. International Union of Crystallography 2010-08-04 /pmc/articles/PMC3007826/ /pubmed/21588577 http://dx.doi.org/10.1107/S1600536810029983 Text en © Zhao et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhao, Lin-xiu
Cui, Jian-lan
Cao, Duan-lin
3-Eth­oxy-2-hy­droxy­benzaldehyde 2,4-di­nitro­phenylhydrazone N,N-di­methyl­formamide monosolvate
title 3-Eth­oxy-2-hy­droxy­benzaldehyde 2,4-di­nitro­phenylhydrazone N,N-di­methyl­formamide monosolvate
title_full 3-Eth­oxy-2-hy­droxy­benzaldehyde 2,4-di­nitro­phenylhydrazone N,N-di­methyl­formamide monosolvate
title_fullStr 3-Eth­oxy-2-hy­droxy­benzaldehyde 2,4-di­nitro­phenylhydrazone N,N-di­methyl­formamide monosolvate
title_full_unstemmed 3-Eth­oxy-2-hy­droxy­benzaldehyde 2,4-di­nitro­phenylhydrazone N,N-di­methyl­formamide monosolvate
title_short 3-Eth­oxy-2-hy­droxy­benzaldehyde 2,4-di­nitro­phenylhydrazone N,N-di­methyl­formamide monosolvate
title_sort 3-eth­oxy-2-hy­droxy­benzaldehyde 2,4-di­nitro­phenylhydrazone n,n-di­methyl­formamide monosolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007826/
https://www.ncbi.nlm.nih.gov/pubmed/21588577
http://dx.doi.org/10.1107/S1600536810029983
work_keys_str_mv AT zhaolinxiu 3ethoxy2hydroxybenzaldehyde24dinitrophenylhydrazonenndimethylformamidemonosolvate
AT cuijianlan 3ethoxy2hydroxybenzaldehyde24dinitrophenylhydrazonenndimethylformamidemonosolvate
AT caoduanlin 3ethoxy2hydroxybenzaldehyde24dinitrophenylhydrazonenndimethylformamidemonosolvate

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