5′-Amino-2-oxo-2′,3′-dihydro­spiro­[indoline-3,7′-thieno[3,2-b]pyran]-6′-carbonitrile 1′,1′-dioxide

In the title compound, C(15)H(11)N(3)O(4)S, the dihedral angle between the mean planes of the dihydro­indol-2-one (r.m.s. deviation = 0.015 Å) and dihydro­thieno[3,2-b]pyran (r.m.s. deviation = 0.011 Å) ring systems is 89.53 (3)°. The crytal packing is consolidated by inter­molecular N—H⋯O and N—H⋯N...

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Detalles Bibliográficos
Autores principales: Shen, Shi-De, Feng, Xiao-Dong, Yang, Wei-Hua, Yao, Chang-Sheng
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007879/
https://www.ncbi.nlm.nih.gov/pubmed/21588769
http://dx.doi.org/10.1107/S1600536810032861
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author Shen, Shi-De
Feng, Xiao-Dong
Yang, Wei-Hua
Yao, Chang-Sheng
author_facet Shen, Shi-De
Feng, Xiao-Dong
Yang, Wei-Hua
Yao, Chang-Sheng
author_sort Shen, Shi-De
collection PubMed
description In the title compound, C(15)H(11)N(3)O(4)S, the dihedral angle between the mean planes of the dihydro­indol-2-one (r.m.s. deviation = 0.015 Å) and dihydro­thieno[3,2-b]pyran (r.m.s. deviation = 0.011 Å) ring systems is 89.53 (3)°. The crytal packing is consolidated by inter­molecular N—H⋯O and N—H⋯N hydrogen bonds, which link the mol­ecules into a two-dimensional network into sheets lying parallel to (100).
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spelling pubmed-30078792010-12-30 5′-Amino-2-oxo-2′,3′-dihydro­spiro­[indoline-3,7′-thieno[3,2-b]pyran]-6′-carbonitrile 1′,1′-dioxide Shen, Shi-De Feng, Xiao-Dong Yang, Wei-Hua Yao, Chang-Sheng Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(15)H(11)N(3)O(4)S, the dihedral angle between the mean planes of the dihydro­indol-2-one (r.m.s. deviation = 0.015 Å) and dihydro­thieno[3,2-b]pyran (r.m.s. deviation = 0.011 Å) ring systems is 89.53 (3)°. The crytal packing is consolidated by inter­molecular N—H⋯O and N—H⋯N hydrogen bonds, which link the mol­ecules into a two-dimensional network into sheets lying parallel to (100). International Union of Crystallography 2010-08-28 /pmc/articles/PMC3007879/ /pubmed/21588769 http://dx.doi.org/10.1107/S1600536810032861 Text en © Shen et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Shen, Shi-De
Feng, Xiao-Dong
Yang, Wei-Hua
Yao, Chang-Sheng
5′-Amino-2-oxo-2′,3′-dihydro­spiro­[indoline-3,7′-thieno[3,2-b]pyran]-6′-carbonitrile 1′,1′-dioxide
title 5′-Amino-2-oxo-2′,3′-dihydro­spiro­[indoline-3,7′-thieno[3,2-b]pyran]-6′-carbonitrile 1′,1′-dioxide
title_full 5′-Amino-2-oxo-2′,3′-dihydro­spiro­[indoline-3,7′-thieno[3,2-b]pyran]-6′-carbonitrile 1′,1′-dioxide
title_fullStr 5′-Amino-2-oxo-2′,3′-dihydro­spiro­[indoline-3,7′-thieno[3,2-b]pyran]-6′-carbonitrile 1′,1′-dioxide
title_full_unstemmed 5′-Amino-2-oxo-2′,3′-dihydro­spiro­[indoline-3,7′-thieno[3,2-b]pyran]-6′-carbonitrile 1′,1′-dioxide
title_short 5′-Amino-2-oxo-2′,3′-dihydro­spiro­[indoline-3,7′-thieno[3,2-b]pyran]-6′-carbonitrile 1′,1′-dioxide
title_sort 5′-amino-2-oxo-2′,3′-dihydro­spiro­[indoline-3,7′-thieno[3,2-b]pyran]-6′-carbonitrile 1′,1′-dioxide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007879/
https://www.ncbi.nlm.nih.gov/pubmed/21588769
http://dx.doi.org/10.1107/S1600536810032861
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AT yaochangsheng 5amino2oxo23dihydrospiroindoline37thieno32bpyran6carbonitrile11dioxide

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