1-(2-Oxo-3,4-dihydro-2H-1,3-benzoxazin-4-yl)urea monohydrate

The organic molecule in the title hydrate, C(9)H(9)N(3)O(3)·H(2)O, was obtained by the condenstation of salicylic aldehyde with urea in acetonitrile. The oxazine ring adopts a slightly distorted sofa conformation, with the N atom deviating from the plane passing through the other atoms of the ring b...

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Detalles Bibliográficos
Autores principales: Kurbanova, Malahat M., Novruzova, Aysel B., Gurbanov, Atash V., Ismaylova, Sheyda R., Maharramov, Abel M.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007927/
https://www.ncbi.nlm.nih.gov/pubmed/21588691
http://dx.doi.org/10.1107/S1600536810032411
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author Kurbanova, Malahat M.
Novruzova, Aysel B.
Gurbanov, Atash V.
Ismaylova, Sheyda R.
Maharramov, Abel M.
author_facet Kurbanova, Malahat M.
Novruzova, Aysel B.
Gurbanov, Atash V.
Ismaylova, Sheyda R.
Maharramov, Abel M.
author_sort Kurbanova, Malahat M.
collection PubMed
description The organic molecule in the title hydrate, C(9)H(9)N(3)O(3)·H(2)O, was obtained by the condenstation of salicylic aldehyde with urea in acetonitrile. The oxazine ring adopts a slightly distorted sofa conformation, with the N atom deviating from the plane passing through the other atoms of the ring by 0.267 (2) Å. The crystal structure displays inter­molecular N—H⋯O and O—H⋯O hydrogen bonding.
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spelling pubmed-30079272010-12-30 1-(2-Oxo-3,4-dihydro-2H-1,3-benzoxazin-4-yl)urea monohydrate Kurbanova, Malahat M. Novruzova, Aysel B. Gurbanov, Atash V. Ismaylova, Sheyda R. Maharramov, Abel M. Acta Crystallogr Sect E Struct Rep Online Organic Papers The organic molecule in the title hydrate, C(9)H(9)N(3)O(3)·H(2)O, was obtained by the condenstation of salicylic aldehyde with urea in acetonitrile. The oxazine ring adopts a slightly distorted sofa conformation, with the N atom deviating from the plane passing through the other atoms of the ring by 0.267 (2) Å. The crystal structure displays inter­molecular N—H⋯O and O—H⋯O hydrogen bonding. International Union of Crystallography 2010-08-18 /pmc/articles/PMC3007927/ /pubmed/21588691 http://dx.doi.org/10.1107/S1600536810032411 Text en © Kurbanova et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Kurbanova, Malahat M.
Novruzova, Aysel B.
Gurbanov, Atash V.
Ismaylova, Sheyda R.
Maharramov, Abel M.
1-(2-Oxo-3,4-dihydro-2H-1,3-benzoxazin-4-yl)urea monohydrate
title 1-(2-Oxo-3,4-dihydro-2H-1,3-benzoxazin-4-yl)urea monohydrate
title_full 1-(2-Oxo-3,4-dihydro-2H-1,3-benzoxazin-4-yl)urea monohydrate
title_fullStr 1-(2-Oxo-3,4-dihydro-2H-1,3-benzoxazin-4-yl)urea monohydrate
title_full_unstemmed 1-(2-Oxo-3,4-dihydro-2H-1,3-benzoxazin-4-yl)urea monohydrate
title_short 1-(2-Oxo-3,4-dihydro-2H-1,3-benzoxazin-4-yl)urea monohydrate
title_sort 1-(2-oxo-3,4-dihydro-2h-1,3-benzoxazin-4-yl)urea monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007927/
https://www.ncbi.nlm.nih.gov/pubmed/21588691
http://dx.doi.org/10.1107/S1600536810032411
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AT gurbanovatashv 12oxo34dihydro2h13benzoxazin4ylureamonohydrate
AT ismaylovasheydar 12oxo34dihydro2h13benzoxazin4ylureamonohydrate
AT maharramovabelm 12oxo34dihydro2h13benzoxazin4ylureamonohydrate

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