2,2′-Bi-1,3,4-thia­diazole-5,5′-diamine tetra­hydrate

In the title compound, C(4)H(4)N(6)S(2)·4H(2)O, the complete organic mol­ecule is generated by crystallographic twofold symmetry and the dihedral angle between the aromatic rings is 10.24 (3)°. In the crystal, inter­molecular N—H⋯N, N—H⋯O, O—H⋯N and O—H⋯O hydrogen bonds and aromatic π–π stacking int...

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Detalles Bibliográficos
Autores principales: Pakawatchai, Chaveng, Saithong, Saowanit
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007951/
https://www.ncbi.nlm.nih.gov/pubmed/21588571
http://dx.doi.org/10.1107/S160053681002996X
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author Pakawatchai, Chaveng
Saithong, Saowanit
author_facet Pakawatchai, Chaveng
Saithong, Saowanit
author_sort Pakawatchai, Chaveng
collection PubMed
description In the title compound, C(4)H(4)N(6)S(2)·4H(2)O, the complete organic mol­ecule is generated by crystallographic twofold symmetry and the dihedral angle between the aromatic rings is 10.24 (3)°. In the crystal, inter­molecular N—H⋯N, N—H⋯O, O—H⋯N and O—H⋯O hydrogen bonds and aromatic π–π stacking inter­actions [centroid–centroid separations = 3.530 (3) and 3.600 (3) Å] are observed.
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spelling pubmed-30079512010-12-30 2,2′-Bi-1,3,4-thia­diazole-5,5′-diamine tetra­hydrate Pakawatchai, Chaveng Saithong, Saowanit Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(4)H(4)N(6)S(2)·4H(2)O, the complete organic mol­ecule is generated by crystallographic twofold symmetry and the dihedral angle between the aromatic rings is 10.24 (3)°. In the crystal, inter­molecular N—H⋯N, N—H⋯O, O—H⋯N and O—H⋯O hydrogen bonds and aromatic π–π stacking inter­actions [centroid–centroid separations = 3.530 (3) and 3.600 (3) Å] are observed. International Union of Crystallography 2010-08-04 /pmc/articles/PMC3007951/ /pubmed/21588571 http://dx.doi.org/10.1107/S160053681002996X Text en © Pakawatchai and Saithong 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Pakawatchai, Chaveng
Saithong, Saowanit
2,2′-Bi-1,3,4-thia­diazole-5,5′-diamine tetra­hydrate
title 2,2′-Bi-1,3,4-thia­diazole-5,5′-diamine tetra­hydrate
title_full 2,2′-Bi-1,3,4-thia­diazole-5,5′-diamine tetra­hydrate
title_fullStr 2,2′-Bi-1,3,4-thia­diazole-5,5′-diamine tetra­hydrate
title_full_unstemmed 2,2′-Bi-1,3,4-thia­diazole-5,5′-diamine tetra­hydrate
title_short 2,2′-Bi-1,3,4-thia­diazole-5,5′-diamine tetra­hydrate
title_sort 2,2′-bi-1,3,4-thia­diazole-5,5′-diamine tetra­hydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007951/
https://www.ncbi.nlm.nih.gov/pubmed/21588571
http://dx.doi.org/10.1107/S160053681002996X
work_keys_str_mv AT pakawatchaichaveng 22bi134thiadiazole55diaminetetrahydrate
AT saithongsaowanit 22bi134thiadiazole55diaminetetrahydrate

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