(E)-1-[(1,3-Dioxan-4-yl)meth­yl]-2-(nitro­methyl­idene)imidazolidine

In the title compound, C(9)H(15)N(3)O(4), the 1,3-dioxane ring displays a chair conformation and the five-membered ring is close to planar (r.m.s. deviation = 0.054 Å). An intra­molecular N—H⋯O hydrogen bond to one of the nitro-group O atoms generates an S(6) ring. In the crystal, inter­molecular N—...

Descripción completa

Detalles Bibliográficos
Autores principales: Tian, Zhongzhen, Dong, Haijun, Li, Dongmei, Wang, Gaolei
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007992/
https://www.ncbi.nlm.nih.gov/pubmed/21588701
http://dx.doi.org/10.1107/S1600536810032691
_version_ 1782194476300632064
author Tian, Zhongzhen
Dong, Haijun
Li, Dongmei
Wang, Gaolei
author_facet Tian, Zhongzhen
Dong, Haijun
Li, Dongmei
Wang, Gaolei
author_sort Tian, Zhongzhen
collection PubMed
description In the title compound, C(9)H(15)N(3)O(4), the 1,3-dioxane ring displays a chair conformation and the five-membered ring is close to planar (r.m.s. deviation = 0.054 Å). An intra­molecular N—H⋯O hydrogen bond to one of the nitro-group O atoms generates an S(6) ring. In the crystal, inter­molecular N—H⋯O hydrogen bonds link the mol­ecules into C(6) chains propagating in [010] and a C—H⋯O link also occurs.
format Text
id pubmed-3007992
institution National Center for Biotechnology Information
language English
publishDate 2010
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-30079922010-12-30 (E)-1-[(1,3-Dioxan-4-yl)meth­yl]-2-(nitro­methyl­idene)imidazolidine Tian, Zhongzhen Dong, Haijun Li, Dongmei Wang, Gaolei Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(9)H(15)N(3)O(4), the 1,3-dioxane ring displays a chair conformation and the five-membered ring is close to planar (r.m.s. deviation = 0.054 Å). An intra­molecular N—H⋯O hydrogen bond to one of the nitro-group O atoms generates an S(6) ring. In the crystal, inter­molecular N—H⋯O hydrogen bonds link the mol­ecules into C(6) chains propagating in [010] and a C—H⋯O link also occurs. International Union of Crystallography 2010-08-21 /pmc/articles/PMC3007992/ /pubmed/21588701 http://dx.doi.org/10.1107/S1600536810032691 Text en © Tian et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Tian, Zhongzhen
Dong, Haijun
Li, Dongmei
Wang, Gaolei
(E)-1-[(1,3-Dioxan-4-yl)meth­yl]-2-(nitro­methyl­idene)imidazolidine
title (E)-1-[(1,3-Dioxan-4-yl)meth­yl]-2-(nitro­methyl­idene)imidazolidine
title_full (E)-1-[(1,3-Dioxan-4-yl)meth­yl]-2-(nitro­methyl­idene)imidazolidine
title_fullStr (E)-1-[(1,3-Dioxan-4-yl)meth­yl]-2-(nitro­methyl­idene)imidazolidine
title_full_unstemmed (E)-1-[(1,3-Dioxan-4-yl)meth­yl]-2-(nitro­methyl­idene)imidazolidine
title_short (E)-1-[(1,3-Dioxan-4-yl)meth­yl]-2-(nitro­methyl­idene)imidazolidine
title_sort (e)-1-[(1,3-dioxan-4-yl)meth­yl]-2-(nitro­methyl­idene)imidazolidine
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007992/
https://www.ncbi.nlm.nih.gov/pubmed/21588701
http://dx.doi.org/10.1107/S1600536810032691
work_keys_str_mv AT tianzhongzhen e113dioxan4ylmethyl2nitromethylideneimidazolidine
AT donghaijun e113dioxan4ylmethyl2nitromethylideneimidazolidine
AT lidongmei e113dioxan4ylmethyl2nitromethylideneimidazolidine
AT wanggaolei e113dioxan4ylmethyl2nitromethylideneimidazolidine

Ejemplares similares