Ethane-1,2-diammonium dibromide: a redetermination at 100 K

In the redetermined [for the previous study, see Søtofte (1976 ▶). Acta Chem. Scand. Ser. A, 30, 309–311] crystal structure of the title compound, C(2)H(10)N(2) (2+)·2Br(−), the H atoms have been located and the hydrogen-bonding scheme is described. The ethane-1,2-diammonium cation lies over a cryst...

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Detalles Bibliográficos
Autores principales: Arderne, Charmaine, Kruger, Gert J.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007993/
https://www.ncbi.nlm.nih.gov/pubmed/21588788
http://dx.doi.org/10.1107/S1600536810033313
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author Arderne, Charmaine
Kruger, Gert J.
author_facet Arderne, Charmaine
Kruger, Gert J.
author_sort Arderne, Charmaine
collection PubMed
description In the redetermined [for the previous study, see Søtofte (1976 ▶). Acta Chem. Scand. Ser. A, 30, 309–311] crystal structure of the title compound, C(2)H(10)N(2) (2+)·2Br(−), the H atoms have been located and the hydrogen-bonding scheme is described. The ethane-1,2-diammonium cation lies over a crystallographic inversion centre and straddles a crystallographic mirror plane with the C and N atoms in special positions. In the crystal, the cations and anions are linked by N—H⋯Br and N—H⋯(Br,Br) hydrogen bonds, which generate various ring and chain motifs including an R (10) (5)(32) loop.
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spelling pubmed-30079932010-12-30 Ethane-1,2-diammonium dibromide: a redetermination at 100 K Arderne, Charmaine Kruger, Gert J. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the redetermined [for the previous study, see Søtofte (1976 ▶). Acta Chem. Scand. Ser. A, 30, 309–311] crystal structure of the title compound, C(2)H(10)N(2) (2+)·2Br(−), the H atoms have been located and the hydrogen-bonding scheme is described. The ethane-1,2-diammonium cation lies over a crystallographic inversion centre and straddles a crystallographic mirror plane with the C and N atoms in special positions. In the crystal, the cations and anions are linked by N—H⋯Br and N—H⋯(Br,Br) hydrogen bonds, which generate various ring and chain motifs including an R (10) (5)(32) loop. International Union of Crystallography 2010-08-28 /pmc/articles/PMC3007993/ /pubmed/21588788 http://dx.doi.org/10.1107/S1600536810033313 Text en © Arderne and Kruger 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Arderne, Charmaine
Kruger, Gert J.
Ethane-1,2-diammonium dibromide: a redetermination at 100 K
title Ethane-1,2-diammonium dibromide: a redetermination at 100 K
title_full Ethane-1,2-diammonium dibromide: a redetermination at 100 K
title_fullStr Ethane-1,2-diammonium dibromide: a redetermination at 100 K
title_full_unstemmed Ethane-1,2-diammonium dibromide: a redetermination at 100 K
title_short Ethane-1,2-diammonium dibromide: a redetermination at 100 K
title_sort ethane-1,2-diammonium dibromide: a redetermination at 100 k
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007993/
https://www.ncbi.nlm.nih.gov/pubmed/21588788
http://dx.doi.org/10.1107/S1600536810033313
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AT krugergertj ethane12diammoniumdibromidearedeterminationat100k

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