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2-Hydroxy-4-methoxybenzaldehyde thiosemicarbazone
The title Schiff base compound, C(9)H(11)N(3)O(2)S, was prepared by the reaction of equimolar quantities of 2-hydroxy-4-methoxybenzaldehyde with thiosemicarbazide in methanol. The molecule adopts a trans configuration with respect to the azomethine group and an intramolecular O—H⋯N hydrogen...
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Formato: | Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2010
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Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3008052/ https://www.ncbi.nlm.nih.gov/pubmed/21588582 http://dx.doi.org/10.1107/S1600536810029594 |
Sumario: | The title Schiff base compound, C(9)H(11)N(3)O(2)S, was prepared by the reaction of equimolar quantities of 2-hydroxy-4-methoxybenzaldehyde with thiosemicarbazide in methanol. The molecule adopts a trans configuration with respect to the azomethine group and an intramolecular O—H⋯N hydrogen bond generates an S(6) ring. In the crystal structure, molecules are linked through intermolecular N—H⋯O and N—H⋯S hydrogen bonds, forming a three-dimensional network. |
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