2-Hy­droxy-4-meth­oxy­benzaldehyde thio­semicarbazone

The title Schiff base compound, C(9)H(11)N(3)O(2)S, was prepared by the reaction of equimolar quanti­ties of 2-hy­droxy-4-meth­oxy­benzaldehyde with thio­semicarbazide in methanol. The mol­ecule adopts a trans configuration with respect to the azo­methine group and an intra­molecular O—H⋯N hydrogen...

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Autor principal: Hao, Yu-Mei
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3008052/
https://www.ncbi.nlm.nih.gov/pubmed/21588582
http://dx.doi.org/10.1107/S1600536810029594
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author Hao, Yu-Mei
author_facet Hao, Yu-Mei
author_sort Hao, Yu-Mei
collection PubMed
description The title Schiff base compound, C(9)H(11)N(3)O(2)S, was prepared by the reaction of equimolar quanti­ties of 2-hy­droxy-4-meth­oxy­benzaldehyde with thio­semicarbazide in methanol. The mol­ecule adopts a trans configuration with respect to the azo­methine group and an intra­molecular O—H⋯N hydrogen bond generates an S(6) ring. In the crystal structure, mol­ecules are linked through inter­molecular N—H⋯O and N—H⋯S hydrogen bonds, forming a three-dimensional network.
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spelling pubmed-30080522010-12-30 2-Hy­droxy-4-meth­oxy­benzaldehyde thio­semicarbazone Hao, Yu-Mei Acta Crystallogr Sect E Struct Rep Online Organic Papers The title Schiff base compound, C(9)H(11)N(3)O(2)S, was prepared by the reaction of equimolar quanti­ties of 2-hy­droxy-4-meth­oxy­benzaldehyde with thio­semicarbazide in methanol. The mol­ecule adopts a trans configuration with respect to the azo­methine group and an intra­molecular O—H⋯N hydrogen bond generates an S(6) ring. In the crystal structure, mol­ecules are linked through inter­molecular N—H⋯O and N—H⋯S hydrogen bonds, forming a three-dimensional network. International Union of Crystallography 2010-08-04 /pmc/articles/PMC3008052/ /pubmed/21588582 http://dx.doi.org/10.1107/S1600536810029594 Text en © Yu-Mei Hao 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Hao, Yu-Mei
2-Hy­droxy-4-meth­oxy­benzaldehyde thio­semicarbazone
title 2-Hy­droxy-4-meth­oxy­benzaldehyde thio­semicarbazone
title_full 2-Hy­droxy-4-meth­oxy­benzaldehyde thio­semicarbazone
title_fullStr 2-Hy­droxy-4-meth­oxy­benzaldehyde thio­semicarbazone
title_full_unstemmed 2-Hy­droxy-4-meth­oxy­benzaldehyde thio­semicarbazone
title_short 2-Hy­droxy-4-meth­oxy­benzaldehyde thio­semicarbazone
title_sort 2-hy­droxy-4-meth­oxy­benzaldehyde thio­semicarbazone
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3008052/
https://www.ncbi.nlm.nih.gov/pubmed/21588582
http://dx.doi.org/10.1107/S1600536810029594
work_keys_str_mv AT haoyumei 2hydroxy4methoxybenzaldehydethiosemicarbazone

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