2,2′,5,5′-Tetra­chloro­benzidine

In the crystal structure of the title compound, C(12)H(8)Cl(4)N(2), mol­ecules lie on crystallographic twofold axes at the centre of the C—C bonds linking the benzene rings, such that the asymmetric unit consists of a half-mol­ecule. The individual mol­ecules participate in inter­molecular N—H⋯N, N—...

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Detalles Bibliográficos
Autores principales: Ugono, Onome, Douglas Jr, Marcel, Rath, Nigam P., Beatty, Alicia M.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3008068/
https://www.ncbi.nlm.nih.gov/pubmed/21588639
http://dx.doi.org/10.1107/S1600536810030886
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author Ugono, Onome
Douglas Jr, Marcel
Rath, Nigam P.
Beatty, Alicia M.
author_facet Ugono, Onome
Douglas Jr, Marcel
Rath, Nigam P.
Beatty, Alicia M.
author_sort Ugono, Onome
collection PubMed
description In the crystal structure of the title compound, C(12)H(8)Cl(4)N(2), mol­ecules lie on crystallographic twofold axes at the centre of the C—C bonds linking the benzene rings, such that the asymmetric unit consists of a half-mol­ecule. The individual mol­ecules participate in inter­molecular N—H⋯N, N—H⋯Cl, C—H⋯Cl and Cl⋯Cl [3.4503 (3) Å] inter­actions.
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spelling pubmed-30080682010-12-30 2,2′,5,5′-Tetra­chloro­benzidine Ugono, Onome Douglas Jr, Marcel Rath, Nigam P. Beatty, Alicia M. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the crystal structure of the title compound, C(12)H(8)Cl(4)N(2), mol­ecules lie on crystallographic twofold axes at the centre of the C—C bonds linking the benzene rings, such that the asymmetric unit consists of a half-mol­ecule. The individual mol­ecules participate in inter­molecular N—H⋯N, N—H⋯Cl, C—H⋯Cl and Cl⋯Cl [3.4503 (3) Å] inter­actions. International Union of Crystallography 2010-08-11 /pmc/articles/PMC3008068/ /pubmed/21588639 http://dx.doi.org/10.1107/S1600536810030886 Text en © Ugono et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Ugono, Onome
Douglas Jr, Marcel
Rath, Nigam P.
Beatty, Alicia M.
2,2′,5,5′-Tetra­chloro­benzidine
title 2,2′,5,5′-Tetra­chloro­benzidine
title_full 2,2′,5,5′-Tetra­chloro­benzidine
title_fullStr 2,2′,5,5′-Tetra­chloro­benzidine
title_full_unstemmed 2,2′,5,5′-Tetra­chloro­benzidine
title_short 2,2′,5,5′-Tetra­chloro­benzidine
title_sort 2,2′,5,5′-tetra­chloro­benzidine
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3008068/
https://www.ncbi.nlm.nih.gov/pubmed/21588639
http://dx.doi.org/10.1107/S1600536810030886
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AT douglasjrmarcel 2255tetrachlorobenzidine
AT rathnigamp 2255tetrachlorobenzidine
AT beattyaliciam 2255tetrachlorobenzidine

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