2-Hydroxy-3-methoxybenzaldehyde 2,4-dinitrophenylhydrazone pyridine monosolvate

The Schiff base molecule of the title compound, C(14)H(12)N(4)O(6)·C(5)H(5)N, was obtained from the condensation reaction of 2-hy­droxy-3-meth­oxy­benzaldehyde and 2,4-dinitro­phenyl­hydrazine. The C=N bond of the Schiff base has a trans arrangement and the dihedral angle between the two benzene rin...

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Detalles Bibliográficos
Autores principales: Zhao, Lin-xiu, Cao, Duan-lin, Cui, Jian-lan
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3008079/
https://www.ncbi.nlm.nih.gov/pubmed/21588576
http://dx.doi.org/10.1107/S1600536810029971
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author Zhao, Lin-xiu
Cao, Duan-lin
Cui, Jian-lan
author_facet Zhao, Lin-xiu
Cao, Duan-lin
Cui, Jian-lan
author_sort Zhao, Lin-xiu
collection PubMed
description The Schiff base molecule of the title compound, C(14)H(12)N(4)O(6)·C(5)H(5)N, was obtained from the condensation reaction of 2-hy­droxy-3-meth­oxy­benzaldehyde and 2,4-dinitro­phenyl­hydrazine. The C=N bond of the Schiff base has a trans arrangement and the dihedral angle between the two benzene rings is 3.49 (10)°. An intra­molecular N—H⋯O hydrogen bond generates an S(6) ring. In the crystal, O—H⋯O hydrogen bonds link the Schiff base mol­ecules.
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spelling pubmed-30080792010-12-30 2-Hydroxy-3-methoxybenzaldehyde 2,4-dinitrophenylhydrazone pyridine monosolvate Zhao, Lin-xiu Cao, Duan-lin Cui, Jian-lan Acta Crystallogr Sect E Struct Rep Online Organic Papers The Schiff base molecule of the title compound, C(14)H(12)N(4)O(6)·C(5)H(5)N, was obtained from the condensation reaction of 2-hy­droxy-3-meth­oxy­benzaldehyde and 2,4-dinitro­phenyl­hydrazine. The C=N bond of the Schiff base has a trans arrangement and the dihedral angle between the two benzene rings is 3.49 (10)°. An intra­molecular N—H⋯O hydrogen bond generates an S(6) ring. In the crystal, O—H⋯O hydrogen bonds link the Schiff base mol­ecules. International Union of Crystallography 2010-08-04 /pmc/articles/PMC3008079/ /pubmed/21588576 http://dx.doi.org/10.1107/S1600536810029971 Text en © Zhao et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhao, Lin-xiu
Cao, Duan-lin
Cui, Jian-lan
2-Hydroxy-3-methoxybenzaldehyde 2,4-dinitrophenylhydrazone pyridine monosolvate
title 2-Hydroxy-3-methoxybenzaldehyde 2,4-dinitrophenylhydrazone pyridine monosolvate
title_full 2-Hydroxy-3-methoxybenzaldehyde 2,4-dinitrophenylhydrazone pyridine monosolvate
title_fullStr 2-Hydroxy-3-methoxybenzaldehyde 2,4-dinitrophenylhydrazone pyridine monosolvate
title_full_unstemmed 2-Hydroxy-3-methoxybenzaldehyde 2,4-dinitrophenylhydrazone pyridine monosolvate
title_short 2-Hydroxy-3-methoxybenzaldehyde 2,4-dinitrophenylhydrazone pyridine monosolvate
title_sort 2-hydroxy-3-methoxybenzaldehyde 2,4-dinitrophenylhydrazone pyridine monosolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3008079/
https://www.ncbi.nlm.nih.gov/pubmed/21588576
http://dx.doi.org/10.1107/S1600536810029971
work_keys_str_mv AT zhaolinxiu 2hydroxy3methoxybenzaldehyde24dinitrophenylhydrazonepyridinemonosolvate
AT caoduanlin 2hydroxy3methoxybenzaldehyde24dinitrophenylhydrazonepyridinemonosolvate
AT cuijianlan 2hydroxy3methoxybenzaldehyde24dinitrophenylhydrazonepyridinemonosolvate

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