2-(4-Chloro­phen­oxy)-N′-[2-(4-chloro­phen­oxy)acet­yl]acetohydrazide monohydrate

In the title compound, C(16)H(14)Cl(2)N(2)O(4)·H(2)O, the hydrazine and water mol­ecules are both located on twofold axes. The C—N—N—C torsion angle is −72.66 (1)° and the dihedral angle between the two benzene rings is 67.33 (1)°. In the crystal, mol­ecules are linked into a layer structure by a co...

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Detalles Bibliográficos
Autores principales: Chen, Ting, Tan, Xiaosong
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009049/
https://www.ncbi.nlm.nih.gov/pubmed/21589016
http://dx.doi.org/10.1107/S160053681004050X
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author Chen, Ting
Tan, Xiaosong
author_facet Chen, Ting
Tan, Xiaosong
author_sort Chen, Ting
collection PubMed
description In the title compound, C(16)H(14)Cl(2)N(2)O(4)·H(2)O, the hydrazine and water mol­ecules are both located on twofold axes. The C—N—N—C torsion angle is −72.66 (1)° and the dihedral angle between the two benzene rings is 67.33 (1)°. In the crystal, mol­ecules are linked into a layer structure by a combination of O—H⋯O, N—H⋯O and C—H⋯O hydrogen bonds. Adjacent layers are linked into a three-dimensional network by Cl⋯Cl inter­actions [3.400 (2) Å]. C—H⋯π inter­actions are also observed.
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spelling pubmed-30090492010-12-30 2-(4-Chloro­phen­oxy)-N′-[2-(4-chloro­phen­oxy)acet­yl]acetohydrazide monohydrate Chen, Ting Tan, Xiaosong Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(16)H(14)Cl(2)N(2)O(4)·H(2)O, the hydrazine and water mol­ecules are both located on twofold axes. The C—N—N—C torsion angle is −72.66 (1)° and the dihedral angle between the two benzene rings is 67.33 (1)°. In the crystal, mol­ecules are linked into a layer structure by a combination of O—H⋯O, N—H⋯O and C—H⋯O hydrogen bonds. Adjacent layers are linked into a three-dimensional network by Cl⋯Cl inter­actions [3.400 (2) Å]. C—H⋯π inter­actions are also observed. International Union of Crystallography 2010-10-20 /pmc/articles/PMC3009049/ /pubmed/21589016 http://dx.doi.org/10.1107/S160053681004050X Text en © Chen and Tan 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Chen, Ting
Tan, Xiaosong
2-(4-Chloro­phen­oxy)-N′-[2-(4-chloro­phen­oxy)acet­yl]acetohydrazide monohydrate
title 2-(4-Chloro­phen­oxy)-N′-[2-(4-chloro­phen­oxy)acet­yl]acetohydrazide monohydrate
title_full 2-(4-Chloro­phen­oxy)-N′-[2-(4-chloro­phen­oxy)acet­yl]acetohydrazide monohydrate
title_fullStr 2-(4-Chloro­phen­oxy)-N′-[2-(4-chloro­phen­oxy)acet­yl]acetohydrazide monohydrate
title_full_unstemmed 2-(4-Chloro­phen­oxy)-N′-[2-(4-chloro­phen­oxy)acet­yl]acetohydrazide monohydrate
title_short 2-(4-Chloro­phen­oxy)-N′-[2-(4-chloro­phen­oxy)acet­yl]acetohydrazide monohydrate
title_sort 2-(4-chloro­phen­oxy)-n′-[2-(4-chloro­phen­oxy)acet­yl]acetohydrazide monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009049/
https://www.ncbi.nlm.nih.gov/pubmed/21589016
http://dx.doi.org/10.1107/S160053681004050X
work_keys_str_mv AT chenting 24chlorophenoxyn24chlorophenoxyacetylacetohydrazidemonohydrate
AT tanxiaosong 24chlorophenoxyn24chlorophenoxyacetylacetohydrazidemonohydrate

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