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1-(4-Methoxybenzylidene)-4-methylthiosemicarbazide
The title compound, C(10)H(13)N(3)OS, was prepared by the reaction of 4-methoxybenzaldehyde and 4-methylthiosemicarbazide. The dihedral angle between the benzene ring and the thiourea unit is 8.64 (7)° and an intramolecular N—H⋯N hydrogen bond generates an S(5) ring. In the crystal, inversion...
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| Formato: | Texto |
| Lenguaje: | English |
| Publicado: |
International Union of Crystallography
2010
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| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009075/ https://www.ncbi.nlm.nih.gov/pubmed/21588938 http://dx.doi.org/10.1107/S1600536810038882 |
| Sumario: | The title compound, C(10)H(13)N(3)OS, was prepared by the reaction of 4-methoxybenzaldehyde and 4-methylthiosemicarbazide. The dihedral angle between the benzene ring and the thiourea unit is 8.64 (7)° and an intramolecular N—H⋯N hydrogen bond generates an S(5) ring. In the crystal, inversion dimers linked by pairs of N—H⋯S hydrogen bonds generate R (2) (2)(8) loops. The dimers are linked into (001) sheets by further N—H⋯S links. |
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