4,4′-Bipyridine–cyclo­hexane-1,2,4,5-tetra­carb­oxy­lic acid (1/1)

In the title 1:1 adduct, C(10)H(8)N(2)·C(10)H(12)O(8), the dihedral angle between the pyridine rings in the 4,4-bipyridine molecule is 8.33 (13)°. In the crystal, the cyclo­hexane-1,2,4,5-tetra­carb­oxy­lic acid mol­ecules inter­act with each other through inter­molecular O—H⋯O hydrogen bonds, formi...

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Autor principal: Liu, Jian-Qiang
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009091/
https://www.ncbi.nlm.nih.gov/pubmed/21588947
http://dx.doi.org/10.1107/S1600536810039024
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author Liu, Jian-Qiang
author_facet Liu, Jian-Qiang
author_sort Liu, Jian-Qiang
collection PubMed
description In the title 1:1 adduct, C(10)H(8)N(2)·C(10)H(12)O(8), the dihedral angle between the pyridine rings in the 4,4-bipyridine molecule is 8.33 (13)°. In the crystal, the cyclo­hexane-1,2,4,5-tetra­carb­oxy­lic acid mol­ecules inter­act with each other through inter­molecular O—H⋯O hydrogen bonds, forming an infinite chain along the a axis, which is further linked perpendicularly by O—H⋯N hydrogen bonds involving bipyridine, resulting in a supra­molecular corrugated sheet parallel to the (110) plane.
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spelling pubmed-30090912010-12-30 4,4′-Bipyridine–cyclo­hexane-1,2,4,5-tetra­carb­oxy­lic acid (1/1) Liu, Jian-Qiang Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title 1:1 adduct, C(10)H(8)N(2)·C(10)H(12)O(8), the dihedral angle between the pyridine rings in the 4,4-bipyridine molecule is 8.33 (13)°. In the crystal, the cyclo­hexane-1,2,4,5-tetra­carb­oxy­lic acid mol­ecules inter­act with each other through inter­molecular O—H⋯O hydrogen bonds, forming an infinite chain along the a axis, which is further linked perpendicularly by O—H⋯N hydrogen bonds involving bipyridine, resulting in a supra­molecular corrugated sheet parallel to the (110) plane. International Union of Crystallography 2010-10-09 /pmc/articles/PMC3009091/ /pubmed/21588947 http://dx.doi.org/10.1107/S1600536810039024 Text en © Jian-Qiang Liu 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Liu, Jian-Qiang
4,4′-Bipyridine–cyclo­hexane-1,2,4,5-tetra­carb­oxy­lic acid (1/1)
title 4,4′-Bipyridine–cyclo­hexane-1,2,4,5-tetra­carb­oxy­lic acid (1/1)
title_full 4,4′-Bipyridine–cyclo­hexane-1,2,4,5-tetra­carb­oxy­lic acid (1/1)
title_fullStr 4,4′-Bipyridine–cyclo­hexane-1,2,4,5-tetra­carb­oxy­lic acid (1/1)
title_full_unstemmed 4,4′-Bipyridine–cyclo­hexane-1,2,4,5-tetra­carb­oxy­lic acid (1/1)
title_short 4,4′-Bipyridine–cyclo­hexane-1,2,4,5-tetra­carb­oxy­lic acid (1/1)
title_sort 4,4′-bipyridine–cyclo­hexane-1,2,4,5-tetra­carb­oxy­lic acid (1/1)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009091/
https://www.ncbi.nlm.nih.gov/pubmed/21588947
http://dx.doi.org/10.1107/S1600536810039024
work_keys_str_mv AT liujianqiang 44bipyridinecyclohexane1245tetracarboxylicacid11

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