3,3-Dichloro-1-(chloro­meth­yl)indolin-2-one

In the title compound, C(9)H(6)Cl(3)NO, the pyrrole ring is almost coplanar with the benzene ring [dihedral angle = 1.90 (9)°], while the Cl—C—N—C torsion angle is 98.78 (17)°. In the crystal, pairs of mol­ecules are inter­connected by pairs of Cl⋯Cl inter­actions [3.564 (5) Å], forming dimers, whic...

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Detalles Bibliográficos
Autores principales: Wang, Yao, Wan, Chong-Qing, Zheng, Tingting, Cao, Sheng-Li
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009249/
https://www.ncbi.nlm.nih.gov/pubmed/21589042
http://dx.doi.org/10.1107/S1600536810040717
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author Wang, Yao
Wan, Chong-Qing
Zheng, Tingting
Cao, Sheng-Li
author_facet Wang, Yao
Wan, Chong-Qing
Zheng, Tingting
Cao, Sheng-Li
author_sort Wang, Yao
collection PubMed
description In the title compound, C(9)H(6)Cl(3)NO, the pyrrole ring is almost coplanar with the benzene ring [dihedral angle = 1.90 (9)°], while the Cl—C—N—C torsion angle is 98.78 (17)°. In the crystal, pairs of mol­ecules are inter­connected by pairs of Cl⋯Cl inter­actions [3.564 (5) Å], forming dimers, which are further peripherally connected through inter­molecular C—H⋯O=C and π–π inter­actions [centroid–centroid distances = 4.134 (7), 4.134 (6) and 4.238 (7) Å], forming a two-dimensional network.
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spelling pubmed-30092492010-12-30 3,3-Dichloro-1-(chloro­meth­yl)indolin-2-one Wang, Yao Wan, Chong-Qing Zheng, Tingting Cao, Sheng-Li Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(9)H(6)Cl(3)NO, the pyrrole ring is almost coplanar with the benzene ring [dihedral angle = 1.90 (9)°], while the Cl—C—N—C torsion angle is 98.78 (17)°. In the crystal, pairs of mol­ecules are inter­connected by pairs of Cl⋯Cl inter­actions [3.564 (5) Å], forming dimers, which are further peripherally connected through inter­molecular C—H⋯O=C and π–π inter­actions [centroid–centroid distances = 4.134 (7), 4.134 (6) and 4.238 (7) Å], forming a two-dimensional network. International Union of Crystallography 2010-10-20 /pmc/articles/PMC3009249/ /pubmed/21589042 http://dx.doi.org/10.1107/S1600536810040717 Text en © Wang et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wang, Yao
Wan, Chong-Qing
Zheng, Tingting
Cao, Sheng-Li
3,3-Dichloro-1-(chloro­meth­yl)indolin-2-one
title 3,3-Dichloro-1-(chloro­meth­yl)indolin-2-one
title_full 3,3-Dichloro-1-(chloro­meth­yl)indolin-2-one
title_fullStr 3,3-Dichloro-1-(chloro­meth­yl)indolin-2-one
title_full_unstemmed 3,3-Dichloro-1-(chloro­meth­yl)indolin-2-one
title_short 3,3-Dichloro-1-(chloro­meth­yl)indolin-2-one
title_sort 3,3-dichloro-1-(chloro­meth­yl)indolin-2-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009249/
https://www.ncbi.nlm.nih.gov/pubmed/21589042
http://dx.doi.org/10.1107/S1600536810040717
work_keys_str_mv AT wangyao 33dichloro1chloromethylindolin2one
AT wanchongqing 33dichloro1chloromethylindolin2one
AT zhengtingting 33dichloro1chloromethylindolin2one
AT caoshengli 33dichloro1chloromethylindolin2one

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