4-Amino­benzoic acid–4,4′-(propane-1,3-diyl)dipyridine (1/1)

In the crystal structure of the title compound, C(13)H(14)N(2)·C(7)H(7)NO(2), the 4,4′-trimethyl­ene-dipyridine (TMDP) mol­ecule displays an approximately planar structure, the maximum atomic deviation excluding H atoms being 0.118 (2) Å and the dihedral angle between the pyridine rings 4.59 (10)°....

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Detalles Bibliográficos
Autores principales: Shen, Fwu Ming, Lush, Shie Fu
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009261/
https://www.ncbi.nlm.nih.gov/pubmed/21588953
http://dx.doi.org/10.1107/S1600536810039528
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author Shen, Fwu Ming
Lush, Shie Fu
author_facet Shen, Fwu Ming
Lush, Shie Fu
author_sort Shen, Fwu Ming
collection PubMed
description In the crystal structure of the title compound, C(13)H(14)N(2)·C(7)H(7)NO(2), the 4,4′-trimethyl­ene-dipyridine (TMDP) mol­ecule displays an approximately planar structure, the maximum atomic deviation excluding H atoms being 0.118 (2) Å and the dihedral angle between the pyridine rings 4.59 (10)°. The TMDP and 4-amino­benzoic acid (ABA) mol­ecules are linked by O—H⋯N and N—H⋯N hydrogen bonding, while ABA mol­ecules are linked by O—H⋯O hydrogen bonding. C—H⋯π interactions are also observed between the methyl­ene groups of TMDP mol­ecules and the benzene rings of ABA mol­ecules.
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spelling pubmed-30092612010-12-30 4-Amino­benzoic acid–4,4′-(propane-1,3-diyl)dipyridine (1/1) Shen, Fwu Ming Lush, Shie Fu Acta Crystallogr Sect E Struct Rep Online Organic Papers In the crystal structure of the title compound, C(13)H(14)N(2)·C(7)H(7)NO(2), the 4,4′-trimethyl­ene-dipyridine (TMDP) mol­ecule displays an approximately planar structure, the maximum atomic deviation excluding H atoms being 0.118 (2) Å and the dihedral angle between the pyridine rings 4.59 (10)°. The TMDP and 4-amino­benzoic acid (ABA) mol­ecules are linked by O—H⋯N and N—H⋯N hydrogen bonding, while ABA mol­ecules are linked by O—H⋯O hydrogen bonding. C—H⋯π interactions are also observed between the methyl­ene groups of TMDP mol­ecules and the benzene rings of ABA mol­ecules. International Union of Crystallography 2010-10-09 /pmc/articles/PMC3009261/ /pubmed/21588953 http://dx.doi.org/10.1107/S1600536810039528 Text en © Shen and Lush 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Shen, Fwu Ming
Lush, Shie Fu
4-Amino­benzoic acid–4,4′-(propane-1,3-diyl)dipyridine (1/1)
title 4-Amino­benzoic acid–4,4′-(propane-1,3-diyl)dipyridine (1/1)
title_full 4-Amino­benzoic acid–4,4′-(propane-1,3-diyl)dipyridine (1/1)
title_fullStr 4-Amino­benzoic acid–4,4′-(propane-1,3-diyl)dipyridine (1/1)
title_full_unstemmed 4-Amino­benzoic acid–4,4′-(propane-1,3-diyl)dipyridine (1/1)
title_short 4-Amino­benzoic acid–4,4′-(propane-1,3-diyl)dipyridine (1/1)
title_sort 4-amino­benzoic acid–4,4′-(propane-1,3-diyl)dipyridine (1/1)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009261/
https://www.ncbi.nlm.nih.gov/pubmed/21588953
http://dx.doi.org/10.1107/S1600536810039528
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