Methyl 4-(1H-benzimidazol-2-yl)benzoate trihydrate

The title compound, C(15)H(12)N(2)O(2)·3H(2)O, has been prepared from the reaction of a Schiff base of benzene-1,2-diamine and iron perchlorate at room temperature. The dihedral angle between the benzimidazole ring and the 4-substituted benzene ring is 0.47 (3)°. Hydrogen bonding involving water mol...

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Detalles Bibliográficos
Autores principales: Gupta, Parna, Mandal, Soumik
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009264/
https://www.ncbi.nlm.nih.gov/pubmed/21588958
http://dx.doi.org/10.1107/S1600536810039188
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author Gupta, Parna
Mandal, Soumik
author_facet Gupta, Parna
Mandal, Soumik
author_sort Gupta, Parna
collection PubMed
description The title compound, C(15)H(12)N(2)O(2)·3H(2)O, has been prepared from the reaction of a Schiff base of benzene-1,2-diamine and iron perchlorate at room temperature. The dihedral angle between the benzimidazole ring and the 4-substituted benzene ring is 0.47 (3)°. Hydrogen bonding involving water mol­ecules, imidazole N, imidazole imine H and ester O atoms stabilizes the crystal structure.
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spelling pubmed-30092642010-12-30 Methyl 4-(1H-benzimidazol-2-yl)benzoate trihydrate Gupta, Parna Mandal, Soumik Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(15)H(12)N(2)O(2)·3H(2)O, has been prepared from the reaction of a Schiff base of benzene-1,2-diamine and iron perchlorate at room temperature. The dihedral angle between the benzimidazole ring and the 4-substituted benzene ring is 0.47 (3)°. Hydrogen bonding involving water mol­ecules, imidazole N, imidazole imine H and ester O atoms stabilizes the crystal structure. International Union of Crystallography 2010-10-09 /pmc/articles/PMC3009264/ /pubmed/21588958 http://dx.doi.org/10.1107/S1600536810039188 Text en © Gupta and Mandal 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Gupta, Parna
Mandal, Soumik
Methyl 4-(1H-benzimidazol-2-yl)benzoate trihydrate
title Methyl 4-(1H-benzimidazol-2-yl)benzoate trihydrate
title_full Methyl 4-(1H-benzimidazol-2-yl)benzoate trihydrate
title_fullStr Methyl 4-(1H-benzimidazol-2-yl)benzoate trihydrate
title_full_unstemmed Methyl 4-(1H-benzimidazol-2-yl)benzoate trihydrate
title_short Methyl 4-(1H-benzimidazol-2-yl)benzoate trihydrate
title_sort methyl 4-(1h-benzimidazol-2-yl)benzoate trihydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009264/
https://www.ncbi.nlm.nih.gov/pubmed/21588958
http://dx.doi.org/10.1107/S1600536810039188
work_keys_str_mv AT guptaparna methyl41hbenzimidazol2ylbenzoatetrihydrate
AT mandalsoumik methyl41hbenzimidazol2ylbenzoatetrihydrate

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