Cargando…

2-(4-Methyl­phen­yl)-2H-indazole

The title compound, C(14)H(12)N(2), was synthesized by the reaction of 4-methyl-N-(2-nitro­benz­yl)aniline with tin(II) chloride dihydrate in ethanol at 313 K. The indazole ring system is almost planar with a dihedral angle of 1.58 (10)° between the rings, whereas the plane of the attached p-tolyl s...

Descripción completa

Detalles Bibliográficos
Autores principales: Zhou, Xingqin, Qin, Xiaofen, Zhang, Jiankang
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009268/
https://www.ncbi.nlm.nih.gov/pubmed/21588941
http://dx.doi.org/10.1107/S1600536810038948
_version_ 1782194647264657408
author Zhou, Xingqin
Qin, Xiaofen
Zhang, Jiankang
author_facet Zhou, Xingqin
Qin, Xiaofen
Zhang, Jiankang
author_sort Zhou, Xingqin
collection PubMed
description The title compound, C(14)H(12)N(2), was synthesized by the reaction of 4-methyl-N-(2-nitro­benz­yl)aniline with tin(II) chloride dihydrate in ethanol at 313 K. The indazole ring system is almost planar with a dihedral angle of 1.58 (10)° between the rings, whereas the plane of the attached p-tolyl substituent shows a dihedral angle of 46.26 (5)° with respect to the indazole core.
format Text
id pubmed-3009268
institution National Center for Biotechnology Information
language English
publishDate 2010
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-30092682010-12-30 2-(4-Methyl­phen­yl)-2H-indazole Zhou, Xingqin Qin, Xiaofen Zhang, Jiankang Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(14)H(12)N(2), was synthesized by the reaction of 4-methyl-N-(2-nitro­benz­yl)aniline with tin(II) chloride dihydrate in ethanol at 313 K. The indazole ring system is almost planar with a dihedral angle of 1.58 (10)° between the rings, whereas the plane of the attached p-tolyl substituent shows a dihedral angle of 46.26 (5)° with respect to the indazole core. International Union of Crystallography 2010-10-09 /pmc/articles/PMC3009268/ /pubmed/21588941 http://dx.doi.org/10.1107/S1600536810038948 Text en © Zhou et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhou, Xingqin
Qin, Xiaofen
Zhang, Jiankang
2-(4-Methyl­phen­yl)-2H-indazole
title 2-(4-Methyl­phen­yl)-2H-indazole
title_full 2-(4-Methyl­phen­yl)-2H-indazole
title_fullStr 2-(4-Methyl­phen­yl)-2H-indazole
title_full_unstemmed 2-(4-Methyl­phen­yl)-2H-indazole
title_short 2-(4-Methyl­phen­yl)-2H-indazole
title_sort 2-(4-methyl­phen­yl)-2h-indazole
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009268/
https://www.ncbi.nlm.nih.gov/pubmed/21588941
http://dx.doi.org/10.1107/S1600536810038948
work_keys_str_mv AT zhouxingqin 24methylphenyl2hindazole
AT qinxiaofen 24methylphenyl2hindazole
AT zhangjiankang 24methylphenyl2hindazole