Cargando…
2-(4-Methylphenyl)-2H-indazole
The title compound, C(14)H(12)N(2), was synthesized by the reaction of 4-methyl-N-(2-nitrobenzyl)aniline with tin(II) chloride dihydrate in ethanol at 313 K. The indazole ring system is almost planar with a dihedral angle of 1.58 (10)° between the rings, whereas the plane of the attached p-tolyl s...
Autores principales: | , , |
---|---|
Formato: | Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2010
|
Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009268/ https://www.ncbi.nlm.nih.gov/pubmed/21588941 http://dx.doi.org/10.1107/S1600536810038948 |
_version_ | 1782194647264657408 |
---|---|
author | Zhou, Xingqin Qin, Xiaofen Zhang, Jiankang |
author_facet | Zhou, Xingqin Qin, Xiaofen Zhang, Jiankang |
author_sort | Zhou, Xingqin |
collection | PubMed |
description | The title compound, C(14)H(12)N(2), was synthesized by the reaction of 4-methyl-N-(2-nitrobenzyl)aniline with tin(II) chloride dihydrate in ethanol at 313 K. The indazole ring system is almost planar with a dihedral angle of 1.58 (10)° between the rings, whereas the plane of the attached p-tolyl substituent shows a dihedral angle of 46.26 (5)° with respect to the indazole core. |
format | Text |
id | pubmed-3009268 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2010 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-30092682010-12-30 2-(4-Methylphenyl)-2H-indazole Zhou, Xingqin Qin, Xiaofen Zhang, Jiankang Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(14)H(12)N(2), was synthesized by the reaction of 4-methyl-N-(2-nitrobenzyl)aniline with tin(II) chloride dihydrate in ethanol at 313 K. The indazole ring system is almost planar with a dihedral angle of 1.58 (10)° between the rings, whereas the plane of the attached p-tolyl substituent shows a dihedral angle of 46.26 (5)° with respect to the indazole core. International Union of Crystallography 2010-10-09 /pmc/articles/PMC3009268/ /pubmed/21588941 http://dx.doi.org/10.1107/S1600536810038948 Text en © Zhou et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Zhou, Xingqin Qin, Xiaofen Zhang, Jiankang 2-(4-Methylphenyl)-2H-indazole |
title | 2-(4-Methylphenyl)-2H-indazole |
title_full | 2-(4-Methylphenyl)-2H-indazole |
title_fullStr | 2-(4-Methylphenyl)-2H-indazole |
title_full_unstemmed | 2-(4-Methylphenyl)-2H-indazole |
title_short | 2-(4-Methylphenyl)-2H-indazole |
title_sort | 2-(4-methylphenyl)-2h-indazole |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009268/ https://www.ncbi.nlm.nih.gov/pubmed/21588941 http://dx.doi.org/10.1107/S1600536810038948 |
work_keys_str_mv | AT zhouxingqin 24methylphenyl2hindazole AT qinxiaofen 24methylphenyl2hindazole AT zhangjiankang 24methylphenyl2hindazole |