1,5-Dimethyl-3-[(3-phenyl-4,5-dihydro-1,2-oxazol-5-yl)meth­yl]-1H-1,5-benzodiazepine-2,4(3H,5H)-dione

The reaction of 3-allyl-1,5-dimethyl-1,5-benzodiazepine-2,4-dione and benzaldoxime leads to the title compound, C(21)H(21)N(3)O(3). The mol­ecular structure is built up from two fused six- and seven-membered rings linked to a chain including a five- and six-membered ring (isoxazoline and phen­yl) vi...

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Autores principales: Dardouri, Rachida, Kandri Rodi, Youssef, Saffon, Nathalie, El Ammari, Lahcen, Essassi, El Mokhtar
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009296/
https://www.ncbi.nlm.nih.gov/pubmed/21589149
http://dx.doi.org/10.1107/S1600536810042972
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author Dardouri, Rachida
Kandri Rodi, Youssef
Saffon, Nathalie
El Ammari, Lahcen
Essassi, El Mokhtar
author_facet Dardouri, Rachida
Kandri Rodi, Youssef
Saffon, Nathalie
El Ammari, Lahcen
Essassi, El Mokhtar
author_sort Dardouri, Rachida
collection PubMed
description The reaction of 3-allyl-1,5-dimethyl-1,5-benzodiazepine-2,4-dione and benzaldoxime leads to the title compound, C(21)H(21)N(3)O(3). The mol­ecular structure is built up from two fused six- and seven-membered rings linked to a chain including a five- and six-membered ring (isoxazoline and phen­yl) via a methyl­ene group. The seven-membered ring displays a boat conformation. The dihedral angle between the two six-membered rings is 74.3 (1)°.
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spelling pubmed-30092962010-12-30 1,5-Dimethyl-3-[(3-phenyl-4,5-dihydro-1,2-oxazol-5-yl)meth­yl]-1H-1,5-benzodiazepine-2,4(3H,5H)-dione Dardouri, Rachida Kandri Rodi, Youssef Saffon, Nathalie El Ammari, Lahcen Essassi, El Mokhtar Acta Crystallogr Sect E Struct Rep Online Organic Papers The reaction of 3-allyl-1,5-dimethyl-1,5-benzodiazepine-2,4-dione and benzaldoxime leads to the title compound, C(21)H(21)N(3)O(3). The mol­ecular structure is built up from two fused six- and seven-membered rings linked to a chain including a five- and six-membered ring (isoxazoline and phen­yl) via a methyl­ene group. The seven-membered ring displays a boat conformation. The dihedral angle between the two six-membered rings is 74.3 (1)°. International Union of Crystallography 2010-10-30 /pmc/articles/PMC3009296/ /pubmed/21589149 http://dx.doi.org/10.1107/S1600536810042972 Text en © Dardouri et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Dardouri, Rachida
Kandri Rodi, Youssef
Saffon, Nathalie
El Ammari, Lahcen
Essassi, El Mokhtar
1,5-Dimethyl-3-[(3-phenyl-4,5-dihydro-1,2-oxazol-5-yl)meth­yl]-1H-1,5-benzodiazepine-2,4(3H,5H)-dione
title 1,5-Dimethyl-3-[(3-phenyl-4,5-dihydro-1,2-oxazol-5-yl)meth­yl]-1H-1,5-benzodiazepine-2,4(3H,5H)-dione
title_full 1,5-Dimethyl-3-[(3-phenyl-4,5-dihydro-1,2-oxazol-5-yl)meth­yl]-1H-1,5-benzodiazepine-2,4(3H,5H)-dione
title_fullStr 1,5-Dimethyl-3-[(3-phenyl-4,5-dihydro-1,2-oxazol-5-yl)meth­yl]-1H-1,5-benzodiazepine-2,4(3H,5H)-dione
title_full_unstemmed 1,5-Dimethyl-3-[(3-phenyl-4,5-dihydro-1,2-oxazol-5-yl)meth­yl]-1H-1,5-benzodiazepine-2,4(3H,5H)-dione
title_short 1,5-Dimethyl-3-[(3-phenyl-4,5-dihydro-1,2-oxazol-5-yl)meth­yl]-1H-1,5-benzodiazepine-2,4(3H,5H)-dione
title_sort 1,5-dimethyl-3-[(3-phenyl-4,5-dihydro-1,2-oxazol-5-yl)meth­yl]-1h-1,5-benzodiazepine-2,4(3h,5h)-dione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009296/
https://www.ncbi.nlm.nih.gov/pubmed/21589149
http://dx.doi.org/10.1107/S1600536810042972
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