N-[11-(4-Chloro­phen­yl)-11,12-dihydro­benzo[c]phenanthridin-6-yl]benzamide

There are two independent mol­ecules in the asymmetric unit of the title compound, C(30)H(21)ClN(2)O, which differ slightly in the orientation of the unsubstituted phenyl ring. Inter­molecular C—H⋯π inter­actions stabilize the crystal structure. The crystal studied was found to be a racemic twin. Th...

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Detalles Bibliográficos
Autores principales: Zhang, Min, Wu, Xiang-Yang, Yang, Liu-Qing
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009300/
https://www.ncbi.nlm.nih.gov/pubmed/21589140
http://dx.doi.org/10.1107/S1600536810043485
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author Zhang, Min
Wu, Xiang-Yang
Yang, Liu-Qing
author_facet Zhang, Min
Wu, Xiang-Yang
Yang, Liu-Qing
author_sort Zhang, Min
collection PubMed
description There are two independent mol­ecules in the asymmetric unit of the title compound, C(30)H(21)ClN(2)O, which differ slightly in the orientation of the unsubstituted phenyl ring. Inter­molecular C—H⋯π inter­actions stabilize the crystal structure. The crystal studied was found to be a racemic twin. The dihedral angles between the substituted phenyl ring and the benzo[c]phenanthridine system are 87.13 (5) and 79.25 (5)° in the two molecules.
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spelling pubmed-30093002010-12-30 N-[11-(4-Chloro­phen­yl)-11,12-dihydro­benzo[c]phenanthridin-6-yl]benzamide Zhang, Min Wu, Xiang-Yang Yang, Liu-Qing Acta Crystallogr Sect E Struct Rep Online Organic Papers There are two independent mol­ecules in the asymmetric unit of the title compound, C(30)H(21)ClN(2)O, which differ slightly in the orientation of the unsubstituted phenyl ring. Inter­molecular C—H⋯π inter­actions stabilize the crystal structure. The crystal studied was found to be a racemic twin. The dihedral angles between the substituted phenyl ring and the benzo[c]phenanthridine system are 87.13 (5) and 79.25 (5)° in the two molecules. International Union of Crystallography 2010-10-31 /pmc/articles/PMC3009300/ /pubmed/21589140 http://dx.doi.org/10.1107/S1600536810043485 Text en © Zhang et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhang, Min
Wu, Xiang-Yang
Yang, Liu-Qing
N-[11-(4-Chloro­phen­yl)-11,12-dihydro­benzo[c]phenanthridin-6-yl]benzamide
title N-[11-(4-Chloro­phen­yl)-11,12-dihydro­benzo[c]phenanthridin-6-yl]benzamide
title_full N-[11-(4-Chloro­phen­yl)-11,12-dihydro­benzo[c]phenanthridin-6-yl]benzamide
title_fullStr N-[11-(4-Chloro­phen­yl)-11,12-dihydro­benzo[c]phenanthridin-6-yl]benzamide
title_full_unstemmed N-[11-(4-Chloro­phen­yl)-11,12-dihydro­benzo[c]phenanthridin-6-yl]benzamide
title_short N-[11-(4-Chloro­phen­yl)-11,12-dihydro­benzo[c]phenanthridin-6-yl]benzamide
title_sort n-[11-(4-chloro­phen­yl)-11,12-dihydro­benzo[c]phenanthridin-6-yl]benzamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009300/
https://www.ncbi.nlm.nih.gov/pubmed/21589140
http://dx.doi.org/10.1107/S1600536810043485
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AT wuxiangyang n114chlorophenyl1112dihydrobenzocphenanthridin6ylbenzamide
AT yangliuqing n114chlorophenyl1112dihydrobenzocphenanthridin6ylbenzamide

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