1,5-Bis[1-(2,4-dihy­droxy­phen­yl)ethyl­idene]carbonohydrazide dimethyl­formamide disolvate

In the title compound, C(17)H(18)N(4)O(5)·2C(3)H(7)NO, two solvent mol­ecules are linked to the main mol­ecule via N—H⋯O and O—H⋯O hydrogen bonds, forming a hydrogen-bonded trimer. Intra­molecular O—H⋯N hydrogen bonds influence the mol­ecular conformation of the main mol­ecule, and the two benzene r...

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Detalles Bibliográficos
Autores principales: He, Qing-Peng, Tan, Bo, Lu, Ze-Hua
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009339/
https://www.ncbi.nlm.nih.gov/pubmed/21589135
http://dx.doi.org/10.1107/S1600536810043151
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author He, Qing-Peng
Tan, Bo
Lu, Ze-Hua
author_facet He, Qing-Peng
Tan, Bo
Lu, Ze-Hua
author_sort He, Qing-Peng
collection PubMed
description In the title compound, C(17)H(18)N(4)O(5)·2C(3)H(7)NO, two solvent mol­ecules are linked to the main mol­ecule via N—H⋯O and O—H⋯O hydrogen bonds, forming a hydrogen-bonded trimer. Intra­molecular O—H⋯N hydrogen bonds influence the mol­ecular conformation of the main mol­ecule, and the two benzene rings form a dihedral angle of 10.55 (18)°. In the crystal, inter­molecular O—H⋯O hydrogen bonds link hydrogen-bonded trimers into ribbons extending along the b axis.
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spelling pubmed-30093392010-12-30 1,5-Bis[1-(2,4-dihy­droxy­phen­yl)ethyl­idene]carbonohydrazide dimethyl­formamide disolvate He, Qing-Peng Tan, Bo Lu, Ze-Hua Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(17)H(18)N(4)O(5)·2C(3)H(7)NO, two solvent mol­ecules are linked to the main mol­ecule via N—H⋯O and O—H⋯O hydrogen bonds, forming a hydrogen-bonded trimer. Intra­molecular O—H⋯N hydrogen bonds influence the mol­ecular conformation of the main mol­ecule, and the two benzene rings form a dihedral angle of 10.55 (18)°. In the crystal, inter­molecular O—H⋯O hydrogen bonds link hydrogen-bonded trimers into ribbons extending along the b axis. International Union of Crystallography 2010-10-30 /pmc/articles/PMC3009339/ /pubmed/21589135 http://dx.doi.org/10.1107/S1600536810043151 Text en © He et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
He, Qing-Peng
Tan, Bo
Lu, Ze-Hua
1,5-Bis[1-(2,4-dihy­droxy­phen­yl)ethyl­idene]carbonohydrazide dimethyl­formamide disolvate
title 1,5-Bis[1-(2,4-dihy­droxy­phen­yl)ethyl­idene]carbonohydrazide dimethyl­formamide disolvate
title_full 1,5-Bis[1-(2,4-dihy­droxy­phen­yl)ethyl­idene]carbonohydrazide dimethyl­formamide disolvate
title_fullStr 1,5-Bis[1-(2,4-dihy­droxy­phen­yl)ethyl­idene]carbonohydrazide dimethyl­formamide disolvate
title_full_unstemmed 1,5-Bis[1-(2,4-dihy­droxy­phen­yl)ethyl­idene]carbonohydrazide dimethyl­formamide disolvate
title_short 1,5-Bis[1-(2,4-dihy­droxy­phen­yl)ethyl­idene]carbonohydrazide dimethyl­formamide disolvate
title_sort 1,5-bis[1-(2,4-dihy­droxy­phen­yl)ethyl­idene]carbonohydrazide dimethyl­formamide disolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009339/
https://www.ncbi.nlm.nih.gov/pubmed/21589135
http://dx.doi.org/10.1107/S1600536810043151
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AT tanbo 15bis124dihydroxyphenylethylidenecarbonohydrazidedimethylformamidedisolvate
AT luzehua 15bis124dihydroxyphenylethylidenecarbonohydrazidedimethylformamidedisolvate

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