Ethyl 4-(furan-2-yl)-6-methyl-2-oxo-1,2,3,4-tetra­hydro­pyrimidine-5-carboxyl­ate

The asymmetric unit of the title compound, C(12)H(14)N(2)O(4), contains two independent mol­ecules. In one independent mol­ecule, the furanyl fragment is rotationally disordered between two orientations in a 0.625 (6):0.375 (6) ratio. In the crystal, inter­molecular pyrimidine–pyrimidinone N—H⋯O hyd...

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Autor principal: Wang, Hong-Yun
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009344/
https://www.ncbi.nlm.nih.gov/pubmed/21589010
http://dx.doi.org/10.1107/S1600536810040456
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author Wang, Hong-Yun
author_facet Wang, Hong-Yun
author_sort Wang, Hong-Yun
collection PubMed
description The asymmetric unit of the title compound, C(12)H(14)N(2)O(4), contains two independent mol­ecules. In one independent mol­ecule, the furanyl fragment is rotationally disordered between two orientations in a 0.625 (6):0.375 (6) ratio. In the crystal, inter­molecular pyrimidine–pyrimidinone N—H⋯O hydrogen bonds link the mol­ecules into centrosymmetric tetra­mers, which are further associated into ribbons extending in [010] via weak inter­molecular pyrimidine–carboxyl N—H⋯O hydrogen bonds.
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spelling pubmed-30093442010-12-30 Ethyl 4-(furan-2-yl)-6-methyl-2-oxo-1,2,3,4-tetra­hydro­pyrimidine-5-carboxyl­ate Wang, Hong-Yun Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(12)H(14)N(2)O(4), contains two independent mol­ecules. In one independent mol­ecule, the furanyl fragment is rotationally disordered between two orientations in a 0.625 (6):0.375 (6) ratio. In the crystal, inter­molecular pyrimidine–pyrimidinone N—H⋯O hydrogen bonds link the mol­ecules into centrosymmetric tetra­mers, which are further associated into ribbons extending in [010] via weak inter­molecular pyrimidine–carboxyl N—H⋯O hydrogen bonds. International Union of Crystallography 2010-10-20 /pmc/articles/PMC3009344/ /pubmed/21589010 http://dx.doi.org/10.1107/S1600536810040456 Text en © Hong-Yun Wang 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wang, Hong-Yun
Ethyl 4-(furan-2-yl)-6-methyl-2-oxo-1,2,3,4-tetra­hydro­pyrimidine-5-carboxyl­ate
title Ethyl 4-(furan-2-yl)-6-methyl-2-oxo-1,2,3,4-tetra­hydro­pyrimidine-5-carboxyl­ate
title_full Ethyl 4-(furan-2-yl)-6-methyl-2-oxo-1,2,3,4-tetra­hydro­pyrimidine-5-carboxyl­ate
title_fullStr Ethyl 4-(furan-2-yl)-6-methyl-2-oxo-1,2,3,4-tetra­hydro­pyrimidine-5-carboxyl­ate
title_full_unstemmed Ethyl 4-(furan-2-yl)-6-methyl-2-oxo-1,2,3,4-tetra­hydro­pyrimidine-5-carboxyl­ate
title_short Ethyl 4-(furan-2-yl)-6-methyl-2-oxo-1,2,3,4-tetra­hydro­pyrimidine-5-carboxyl­ate
title_sort ethyl 4-(furan-2-yl)-6-methyl-2-oxo-1,2,3,4-tetra­hydro­pyrimidine-5-carboxyl­ate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009344/
https://www.ncbi.nlm.nih.gov/pubmed/21589010
http://dx.doi.org/10.1107/S1600536810040456
work_keys_str_mv AT wanghongyun ethyl4furan2yl6methyl2oxo1234tetrahydropyrimidine5carboxylate

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