4-Chloro-N′-(4-meth­oxy­benzyl­idene)benzohydrazide methanol monosolvate

The title compound, C(15)H(13)ClN(2)O(2)·CH(4)O, consists of a 4-chloro-N′-(4-meth­oxy­benzyl­idene)benzohydrazide (CMB) mol­ecule and a methanol mol­ecule of crystallization. It was obtained by the condensation of 4-meth­oxy­benzaldehyde with 4-chloro­benzohydrazide. In the CMB mol­ecule, the dihed...

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Detalles Bibliográficos
Autores principales: Huang, Hai-Tao, Wu, Hong-Yuan
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009357/
https://www.ncbi.nlm.nih.gov/pubmed/21588939
http://dx.doi.org/10.1107/S1600536810038857
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author Huang, Hai-Tao
Wu, Hong-Yuan
author_facet Huang, Hai-Tao
Wu, Hong-Yuan
author_sort Huang, Hai-Tao
collection PubMed
description The title compound, C(15)H(13)ClN(2)O(2)·CH(4)O, consists of a 4-chloro-N′-(4-meth­oxy­benzyl­idene)benzohydrazide (CMB) mol­ecule and a methanol mol­ecule of crystallization. It was obtained by the condensation of 4-meth­oxy­benzaldehyde with 4-chloro­benzohydrazide. In the CMB mol­ecule, the dihedral angle between the two benzene rings is 50.1 (3)°. The methanol mol­ecule is linked to the CMB mol­ecule through O—H⋯O and O—H⋯N hydrogen bonds. In the crystal, CMB mol­ecules are linked through inter­molecular N—H⋯O hydrogen bonds, involving the methanol mol­ecule, forming chains propagating along [010].
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spelling pubmed-30093572010-12-30 4-Chloro-N′-(4-meth­oxy­benzyl­idene)benzohydrazide methanol monosolvate Huang, Hai-Tao Wu, Hong-Yuan Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(15)H(13)ClN(2)O(2)·CH(4)O, consists of a 4-chloro-N′-(4-meth­oxy­benzyl­idene)benzohydrazide (CMB) mol­ecule and a methanol mol­ecule of crystallization. It was obtained by the condensation of 4-meth­oxy­benzaldehyde with 4-chloro­benzohydrazide. In the CMB mol­ecule, the dihedral angle between the two benzene rings is 50.1 (3)°. The methanol mol­ecule is linked to the CMB mol­ecule through O—H⋯O and O—H⋯N hydrogen bonds. In the crystal, CMB mol­ecules are linked through inter­molecular N—H⋯O hydrogen bonds, involving the methanol mol­ecule, forming chains propagating along [010]. International Union of Crystallography 2010-10-09 /pmc/articles/PMC3009357/ /pubmed/21588939 http://dx.doi.org/10.1107/S1600536810038857 Text en © Huang and Wu 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Huang, Hai-Tao
Wu, Hong-Yuan
4-Chloro-N′-(4-meth­oxy­benzyl­idene)benzohydrazide methanol monosolvate
title 4-Chloro-N′-(4-meth­oxy­benzyl­idene)benzohydrazide methanol monosolvate
title_full 4-Chloro-N′-(4-meth­oxy­benzyl­idene)benzohydrazide methanol monosolvate
title_fullStr 4-Chloro-N′-(4-meth­oxy­benzyl­idene)benzohydrazide methanol monosolvate
title_full_unstemmed 4-Chloro-N′-(4-meth­oxy­benzyl­idene)benzohydrazide methanol monosolvate
title_short 4-Chloro-N′-(4-meth­oxy­benzyl­idene)benzohydrazide methanol monosolvate
title_sort 4-chloro-n′-(4-meth­oxy­benzyl­idene)benzohydrazide methanol monosolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009357/
https://www.ncbi.nlm.nih.gov/pubmed/21588939
http://dx.doi.org/10.1107/S1600536810038857
work_keys_str_mv AT huanghaitao 4chloron4methoxybenzylidenebenzohydrazidemethanolmonosolvate
AT wuhongyuan 4chloron4methoxybenzylidenebenzohydrazidemethanolmonosolvate

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