2-[3-(1H-Benzimidazol-2-yl)prop­yl]-1H-benzimidazol-3-ium 3,5-dicarb­oxy­benzoate–benzene-1,3,5-tricarb­oxy­lic acid–water (1/1/1)

The title compound, C(17)H(17)N(4) (+)·C(9)H(5)O(6) (−)·C(9)H(6)O(6)·H(2)O, contains a protonated 2,2′-(1,3-propanedi­yl)bis­(1H-benzimidazole) cation, a deprotonated benzene-1,3,5-tricarb­oxy­lic acid anion, a neutral benzene-1,3,5-tricarb­oxy­lic acid mol­ecule and a water mol­ecule, which are lin...

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Detalles Bibliográficos
Autores principales: Feng, Guo-dong, Jiang, Luan
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009361/
https://www.ncbi.nlm.nih.gov/pubmed/21588940
http://dx.doi.org/10.1107/S1600536810039139
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author Feng, Guo-dong
Jiang, Luan
author_facet Feng, Guo-dong
Jiang, Luan
author_sort Feng, Guo-dong
collection PubMed
description The title compound, C(17)H(17)N(4) (+)·C(9)H(5)O(6) (−)·C(9)H(6)O(6)·H(2)O, contains a protonated 2,2′-(1,3-propanedi­yl)bis­(1H-benzimidazole) cation, a deprotonated benzene-1,3,5-tricarb­oxy­lic acid anion, a neutral benzene-1,3,5-tricarb­oxy­lic acid mol­ecule and a water mol­ecule, which are linked together through N—H⋯O, O—H⋯O and weak C—H⋯O hydrogen bonds into almost double sheets parallel to (4[Image: see text] [Image: see text]). These hydrogen-bonded sheets are packed in the crystal with the formation of centrosymmetric voids of 25.5 Å(3), which are filled by the water mol­ecules.
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spelling pubmed-30093612010-12-30 2-[3-(1H-Benzimidazol-2-yl)prop­yl]-1H-benzimidazol-3-ium 3,5-dicarb­oxy­benzoate–benzene-1,3,5-tricarb­oxy­lic acid–water (1/1/1) Feng, Guo-dong Jiang, Luan Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(17)H(17)N(4) (+)·C(9)H(5)O(6) (−)·C(9)H(6)O(6)·H(2)O, contains a protonated 2,2′-(1,3-propanedi­yl)bis­(1H-benzimidazole) cation, a deprotonated benzene-1,3,5-tricarb­oxy­lic acid anion, a neutral benzene-1,3,5-tricarb­oxy­lic acid mol­ecule and a water mol­ecule, which are linked together through N—H⋯O, O—H⋯O and weak C—H⋯O hydrogen bonds into almost double sheets parallel to (4[Image: see text] [Image: see text]). These hydrogen-bonded sheets are packed in the crystal with the formation of centrosymmetric voids of 25.5 Å(3), which are filled by the water mol­ecules. International Union of Crystallography 2010-10-09 /pmc/articles/PMC3009361/ /pubmed/21588940 http://dx.doi.org/10.1107/S1600536810039139 Text en © Feng and Jiang 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Feng, Guo-dong
Jiang, Luan
2-[3-(1H-Benzimidazol-2-yl)prop­yl]-1H-benzimidazol-3-ium 3,5-dicarb­oxy­benzoate–benzene-1,3,5-tricarb­oxy­lic acid–water (1/1/1)
title 2-[3-(1H-Benzimidazol-2-yl)prop­yl]-1H-benzimidazol-3-ium 3,5-dicarb­oxy­benzoate–benzene-1,3,5-tricarb­oxy­lic acid–water (1/1/1)
title_full 2-[3-(1H-Benzimidazol-2-yl)prop­yl]-1H-benzimidazol-3-ium 3,5-dicarb­oxy­benzoate–benzene-1,3,5-tricarb­oxy­lic acid–water (1/1/1)
title_fullStr 2-[3-(1H-Benzimidazol-2-yl)prop­yl]-1H-benzimidazol-3-ium 3,5-dicarb­oxy­benzoate–benzene-1,3,5-tricarb­oxy­lic acid–water (1/1/1)
title_full_unstemmed 2-[3-(1H-Benzimidazol-2-yl)prop­yl]-1H-benzimidazol-3-ium 3,5-dicarb­oxy­benzoate–benzene-1,3,5-tricarb­oxy­lic acid–water (1/1/1)
title_short 2-[3-(1H-Benzimidazol-2-yl)prop­yl]-1H-benzimidazol-3-ium 3,5-dicarb­oxy­benzoate–benzene-1,3,5-tricarb­oxy­lic acid–water (1/1/1)
title_sort 2-[3-(1h-benzimidazol-2-yl)prop­yl]-1h-benzimidazol-3-ium 3,5-dicarb­oxy­benzoate–benzene-1,3,5-tricarb­oxy­lic acid–water (1/1/1)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3009361/
https://www.ncbi.nlm.nih.gov/pubmed/21588940
http://dx.doi.org/10.1107/S1600536810039139
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