(E)-N′-(2,4-Dichloro­benzyl­idene)-3-nitro­benzohydrazide

The title compound, C(14)H(9)Cl(2)N(3)O(3), was prepared by the reaction of 3-nitro­benzohydrazide with 2,4-dichloro­benzalde­hyde. The mol­ecule adopts an E configuration about the C=N bond. The dihedral angle between the two benzene rings is 4.6 (2)°. In the crystal, the hydrazone mol­ecules are l...

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Detalles Bibliográficos
Autores principales: Mao, Fu-Lin, Dai, Chun-Hua
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3011430/
https://www.ncbi.nlm.nih.gov/pubmed/21589629
http://dx.doi.org/10.1107/S1600536810049470
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author Mao, Fu-Lin
Dai, Chun-Hua
author_facet Mao, Fu-Lin
Dai, Chun-Hua
author_sort Mao, Fu-Lin
collection PubMed
description The title compound, C(14)H(9)Cl(2)N(3)O(3), was prepared by the reaction of 3-nitro­benzohydrazide with 2,4-dichloro­benzalde­hyde. The mol­ecule adopts an E configuration about the C=N bond. The dihedral angle between the two benzene rings is 4.6 (2)°. In the crystal, the hydrazone mol­ecules are linked through inter­molecular N—H⋯O hydrogen bonds, forming chains along the c axis.
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spelling pubmed-30114302010-12-30 (E)-N′-(2,4-Dichloro­benzyl­idene)-3-nitro­benzohydrazide Mao, Fu-Lin Dai, Chun-Hua Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(14)H(9)Cl(2)N(3)O(3), was prepared by the reaction of 3-nitro­benzohydrazide with 2,4-dichloro­benzalde­hyde. The mol­ecule adopts an E configuration about the C=N bond. The dihedral angle between the two benzene rings is 4.6 (2)°. In the crystal, the hydrazone mol­ecules are linked through inter­molecular N—H⋯O hydrogen bonds, forming chains along the c axis. International Union of Crystallography 2010-11-30 /pmc/articles/PMC3011430/ /pubmed/21589629 http://dx.doi.org/10.1107/S1600536810049470 Text en © Mao and Dai 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Mao, Fu-Lin
Dai, Chun-Hua
(E)-N′-(2,4-Dichloro­benzyl­idene)-3-nitro­benzohydrazide
title (E)-N′-(2,4-Dichloro­benzyl­idene)-3-nitro­benzohydrazide
title_full (E)-N′-(2,4-Dichloro­benzyl­idene)-3-nitro­benzohydrazide
title_fullStr (E)-N′-(2,4-Dichloro­benzyl­idene)-3-nitro­benzohydrazide
title_full_unstemmed (E)-N′-(2,4-Dichloro­benzyl­idene)-3-nitro­benzohydrazide
title_short (E)-N′-(2,4-Dichloro­benzyl­idene)-3-nitro­benzohydrazide
title_sort (e)-n′-(2,4-dichloro­benzyl­idene)-3-nitro­benzohydrazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3011430/
https://www.ncbi.nlm.nih.gov/pubmed/21589629
http://dx.doi.org/10.1107/S1600536810049470
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AT daichunhua en24dichlorobenzylidene3nitrobenzohydrazide

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