(3E,5E)-3,5-Bis(4-hy­droxy-3,5-di­methoxy­benzyl­idene)oxan-4-one monohydrate

In the title compound, C(23)H(24)O(8)·H(2)O, the six-membered ring of the oxan-4-one (tetra­hydro­pyran-4-one) ring displays an envelope conformation with the heterocyclic O atom at the flap position. The dihedral angles between the terminal benzene rings is 37.23 (10)°. Classical intermolecular O—H...

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Detalles Bibliográficos
Autores principales: Du, Zhi-Yun, Huang, Hua-Rong, Lu, Yu-Jun, Zhang, Kun, Fang, Yan-Xiong
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3011648/
https://www.ncbi.nlm.nih.gov/pubmed/21589608
http://dx.doi.org/10.1107/S1600536810041930
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author Du, Zhi-Yun
Huang, Hua-Rong
Lu, Yu-Jun
Zhang, Kun
Fang, Yan-Xiong
author_facet Du, Zhi-Yun
Huang, Hua-Rong
Lu, Yu-Jun
Zhang, Kun
Fang, Yan-Xiong
author_sort Du, Zhi-Yun
collection PubMed
description In the title compound, C(23)H(24)O(8)·H(2)O, the six-membered ring of the oxan-4-one (tetra­hydro­pyran-4-one) ring displays an envelope conformation with the heterocyclic O atom at the flap position. The dihedral angles between the terminal benzene rings is 37.23 (10)°. Classical intermolecular O—H⋯O and weak C—H⋯O hydrogen bonds are present in the crystal structure.
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spelling pubmed-30116482010-12-30 (3E,5E)-3,5-Bis(4-hy­droxy-3,5-di­methoxy­benzyl­idene)oxan-4-one monohydrate Du, Zhi-Yun Huang, Hua-Rong Lu, Yu-Jun Zhang, Kun Fang, Yan-Xiong Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(23)H(24)O(8)·H(2)O, the six-membered ring of the oxan-4-one (tetra­hydro­pyran-4-one) ring displays an envelope conformation with the heterocyclic O atom at the flap position. The dihedral angles between the terminal benzene rings is 37.23 (10)°. Classical intermolecular O—H⋯O and weak C—H⋯O hydrogen bonds are present in the crystal structure. International Union of Crystallography 2010-11-27 /pmc/articles/PMC3011648/ /pubmed/21589608 http://dx.doi.org/10.1107/S1600536810041930 Text en © Du et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Du, Zhi-Yun
Huang, Hua-Rong
Lu, Yu-Jun
Zhang, Kun
Fang, Yan-Xiong
(3E,5E)-3,5-Bis(4-hy­droxy-3,5-di­methoxy­benzyl­idene)oxan-4-one monohydrate
title (3E,5E)-3,5-Bis(4-hy­droxy-3,5-di­methoxy­benzyl­idene)oxan-4-one monohydrate
title_full (3E,5E)-3,5-Bis(4-hy­droxy-3,5-di­methoxy­benzyl­idene)oxan-4-one monohydrate
title_fullStr (3E,5E)-3,5-Bis(4-hy­droxy-3,5-di­methoxy­benzyl­idene)oxan-4-one monohydrate
title_full_unstemmed (3E,5E)-3,5-Bis(4-hy­droxy-3,5-di­methoxy­benzyl­idene)oxan-4-one monohydrate
title_short (3E,5E)-3,5-Bis(4-hy­droxy-3,5-di­methoxy­benzyl­idene)oxan-4-one monohydrate
title_sort (3e,5e)-3,5-bis(4-hy­droxy-3,5-di­methoxy­benzyl­idene)oxan-4-one monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3011648/
https://www.ncbi.nlm.nih.gov/pubmed/21589608
http://dx.doi.org/10.1107/S1600536810041930
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