1,1′-(p-Phenyl­enedimethyl­idene)diimidazol-3-ium bis­{2-[(2-carb­oxy­phen­yl)disulfan­yl]benzoate} dihydrate

The title salt, C(14)H(16)N(4) (2+)·2C(14)H(9)O(4)S(2) (−)·2H(2)O, was obtained by the co-crystalization of 2,2′-dithio­dibenzoic acid with 1,4-bis­(imidazol-1-ylmeth­yl)benzene. It consists of 2-[(2-carb­oxy­phen­yl)disulfan­yl]benzoate anions, centrosymmetric 1,1′-(p-phenyl­enedimethyl­idene)diimi...

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Detalles Bibliográficos
Autores principales: Liu, Zhengming, Liu, Qiang, Yuan, Limin, Liu, Wenlong
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3011651/
https://www.ncbi.nlm.nih.gov/pubmed/21589520
http://dx.doi.org/10.1107/S1600536810047021
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author Liu, Zhengming
Liu, Qiang
Yuan, Limin
Liu, Wenlong
author_facet Liu, Zhengming
Liu, Qiang
Yuan, Limin
Liu, Wenlong
author_sort Liu, Zhengming
collection PubMed
description The title salt, C(14)H(16)N(4) (2+)·2C(14)H(9)O(4)S(2) (−)·2H(2)O, was obtained by the co-crystalization of 2,2′-dithio­dibenzoic acid with 1,4-bis­(imidazol-1-ylmeth­yl)benzene. It consists of 2-[(2-carb­oxy­phen­yl)disulfan­yl]benzoate anions, centrosymmetric 1,1′-(p-phenyl­enedimethyl­idene)diimidazol-3-ium cations and water mol­ecules. O—H⋯O, O—H⋯S and N—H⋯O hydrogen-bonding inter­actions among the components lead to the formation of a three-dimensional network.
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spelling pubmed-30116512010-12-30 1,1′-(p-Phenyl­enedimethyl­idene)diimidazol-3-ium bis­{2-[(2-carb­oxy­phen­yl)disulfan­yl]benzoate} dihydrate Liu, Zhengming Liu, Qiang Yuan, Limin Liu, Wenlong Acta Crystallogr Sect E Struct Rep Online Organic Papers The title salt, C(14)H(16)N(4) (2+)·2C(14)H(9)O(4)S(2) (−)·2H(2)O, was obtained by the co-crystalization of 2,2′-dithio­dibenzoic acid with 1,4-bis­(imidazol-1-ylmeth­yl)benzene. It consists of 2-[(2-carb­oxy­phen­yl)disulfan­yl]benzoate anions, centrosymmetric 1,1′-(p-phenyl­enedimethyl­idene)diimidazol-3-ium cations and water mol­ecules. O—H⋯O, O—H⋯S and N—H⋯O hydrogen-bonding inter­actions among the components lead to the formation of a three-dimensional network. International Union of Crystallography 2010-11-20 /pmc/articles/PMC3011651/ /pubmed/21589520 http://dx.doi.org/10.1107/S1600536810047021 Text en © Liu et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Liu, Zhengming
Liu, Qiang
Yuan, Limin
Liu, Wenlong
1,1′-(p-Phenyl­enedimethyl­idene)diimidazol-3-ium bis­{2-[(2-carb­oxy­phen­yl)disulfan­yl]benzoate} dihydrate
title 1,1′-(p-Phenyl­enedimethyl­idene)diimidazol-3-ium bis­{2-[(2-carb­oxy­phen­yl)disulfan­yl]benzoate} dihydrate
title_full 1,1′-(p-Phenyl­enedimethyl­idene)diimidazol-3-ium bis­{2-[(2-carb­oxy­phen­yl)disulfan­yl]benzoate} dihydrate
title_fullStr 1,1′-(p-Phenyl­enedimethyl­idene)diimidazol-3-ium bis­{2-[(2-carb­oxy­phen­yl)disulfan­yl]benzoate} dihydrate
title_full_unstemmed 1,1′-(p-Phenyl­enedimethyl­idene)diimidazol-3-ium bis­{2-[(2-carb­oxy­phen­yl)disulfan­yl]benzoate} dihydrate
title_short 1,1′-(p-Phenyl­enedimethyl­idene)diimidazol-3-ium bis­{2-[(2-carb­oxy­phen­yl)disulfan­yl]benzoate} dihydrate
title_sort 1,1′-(p-phenyl­enedimethyl­idene)diimidazol-3-ium bis­{2-[(2-carb­oxy­phen­yl)disulfan­yl]benzoate} dihydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3011651/
https://www.ncbi.nlm.nih.gov/pubmed/21589520
http://dx.doi.org/10.1107/S1600536810047021
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AT liuqiang 11pphenylenedimethylidenediimidazol3iumbis22carboxyphenyldisulfanylbenzoatedihydrate
AT yuanlimin 11pphenylenedimethylidenediimidazol3iumbis22carboxyphenyldisulfanylbenzoatedihydrate
AT liuwenlong 11pphenylenedimethylidenediimidazol3iumbis22carboxyphenyldisulfanylbenzoatedihydrate

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