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(2Z)-4-[(2-Hy­droxy­phen­yl)carbamo­yl]prop-2-enoic acid

In the title compound, C(10)H(9)NO(4), the 2-hy­droxy­anilinic and the 4-oxobut-2-enoic acid groups are almost planar, with r.m.s. deviations of 0.0086 and 0.0262 Å, respectively. The dihedral angle between the two groups is 6.65 (1)°. Intra­molecular N—H⋯O, C—H⋯O and O—H⋯O hydrogen bonds form S(5),...

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Detalles Bibliográficos
Autores principales: Shah, Farooq Ali, Ali, Saqib, Tahir, M. Nawaz, Ahmed, Sajjad
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3011684/
https://www.ncbi.nlm.nih.gov/pubmed/21589468
http://dx.doi.org/10.1107/S1600536810045496
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author Shah, Farooq Ali
Ali, Saqib
Tahir, M. Nawaz
Ahmed, Sajjad
author_facet Shah, Farooq Ali
Ali, Saqib
Tahir, M. Nawaz
Ahmed, Sajjad
author_sort Shah, Farooq Ali
collection PubMed
description In the title compound, C(10)H(9)NO(4), the 2-hy­droxy­anilinic and the 4-oxobut-2-enoic acid groups are almost planar, with r.m.s. deviations of 0.0086 and 0.0262 Å, respectively. The dihedral angle between the two groups is 6.65 (1)°. Intra­molecular N—H⋯O, C—H⋯O and O—H⋯O hydrogen bonds form S(5), S(6) and S(7) ring motifs. In the crystal, the mol­ecules are dimerized due to C—H⋯O and O—H⋯O inter­molecular hydrogen bonds, with R (2) (2)(8) ring motifs. The dimers are inter­linked into polymeric chains along [010] with R (4) (3)(13) ring motifs by C—H⋯O, N—H⋯O and O—H⋯O hydrogen bonds.
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spelling pubmed-30116842010-12-30 (2Z)-4-[(2-Hy­droxy­phen­yl)carbamo­yl]prop-2-enoic acid Shah, Farooq Ali Ali, Saqib Tahir, M. Nawaz Ahmed, Sajjad Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(10)H(9)NO(4), the 2-hy­droxy­anilinic and the 4-oxobut-2-enoic acid groups are almost planar, with r.m.s. deviations of 0.0086 and 0.0262 Å, respectively. The dihedral angle between the two groups is 6.65 (1)°. Intra­molecular N—H⋯O, C—H⋯O and O—H⋯O hydrogen bonds form S(5), S(6) and S(7) ring motifs. In the crystal, the mol­ecules are dimerized due to C—H⋯O and O—H⋯O inter­molecular hydrogen bonds, with R (2) (2)(8) ring motifs. The dimers are inter­linked into polymeric chains along [010] with R (4) (3)(13) ring motifs by C—H⋯O, N—H⋯O and O—H⋯O hydrogen bonds. International Union of Crystallography 2010-11-13 /pmc/articles/PMC3011684/ /pubmed/21589468 http://dx.doi.org/10.1107/S1600536810045496 Text en © Shah et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Shah, Farooq Ali
Ali, Saqib
Tahir, M. Nawaz
Ahmed, Sajjad
(2Z)-4-[(2-Hy­droxy­phen­yl)carbamo­yl]prop-2-enoic acid
title (2Z)-4-[(2-Hy­droxy­phen­yl)carbamo­yl]prop-2-enoic acid
title_full (2Z)-4-[(2-Hy­droxy­phen­yl)carbamo­yl]prop-2-enoic acid
title_fullStr (2Z)-4-[(2-Hy­droxy­phen­yl)carbamo­yl]prop-2-enoic acid
title_full_unstemmed (2Z)-4-[(2-Hy­droxy­phen­yl)carbamo­yl]prop-2-enoic acid
title_short (2Z)-4-[(2-Hy­droxy­phen­yl)carbamo­yl]prop-2-enoic acid
title_sort (2z)-4-[(2-hy­droxy­phen­yl)carbamo­yl]prop-2-enoic acid
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3011684/
https://www.ncbi.nlm.nih.gov/pubmed/21589468
http://dx.doi.org/10.1107/S1600536810045496
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