[(Pyrrolidin-1-yl)carbothio­ylsulfan­yl]methyl pyrrolidine-1-carbodithio­ate

The title compound, C(11)H(18)N(2)S(4), was unexpectedly obtained during studies on the reactivity of the complex tris­(acac-κ(2) O,O′)gallium(III) (acac is acetyl­acetonate) with C(4)H(8)NCS(2)H in dichloro­methane. The title compound shows disordered two pyrrolidine rings with major and minor occu...

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Autores principales: Chou, Wei-Lung, Yih, Kuang-Hway, Lee, Gene-Hsiang, Huang, Yen-Hsiang, Wang, Hsiao-Fen
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3011744/
https://www.ncbi.nlm.nih.gov/pubmed/21589487
http://dx.doi.org/10.1107/S1600536810046027
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author Chou, Wei-Lung
Yih, Kuang-Hway
Lee, Gene-Hsiang
Huang, Yen-Hsiang
Wang, Hsiao-Fen
author_facet Chou, Wei-Lung
Yih, Kuang-Hway
Lee, Gene-Hsiang
Huang, Yen-Hsiang
Wang, Hsiao-Fen
author_sort Chou, Wei-Lung
collection PubMed
description The title compound, C(11)H(18)N(2)S(4), was unexpectedly obtained during studies on the reactivity of the complex tris­(acac-κ(2) O,O′)gallium(III) (acac is acetyl­acetonate) with C(4)H(8)NCS(2)H in dichloro­methane. The title compound shows disordered two pyrrolidine rings with major and minor occupancies of 0.546 (4) and 0.454 (4). Two (pyrrolidin-1-yl)carbothio­ylsulfanyl units are linked together through a methyl­ene C atom and weak C—H⋯S inter­actions are found.
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spelling pubmed-30117442010-12-30 [(Pyrrolidin-1-yl)carbothio­ylsulfan­yl]methyl pyrrolidine-1-carbodithio­ate Chou, Wei-Lung Yih, Kuang-Hway Lee, Gene-Hsiang Huang, Yen-Hsiang Wang, Hsiao-Fen Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(11)H(18)N(2)S(4), was unexpectedly obtained during studies on the reactivity of the complex tris­(acac-κ(2) O,O′)gallium(III) (acac is acetyl­acetonate) with C(4)H(8)NCS(2)H in dichloro­methane. The title compound shows disordered two pyrrolidine rings with major and minor occupancies of 0.546 (4) and 0.454 (4). Two (pyrrolidin-1-yl)carbothio­ylsulfanyl units are linked together through a methyl­ene C atom and weak C—H⋯S inter­actions are found. International Union of Crystallography 2010-11-17 /pmc/articles/PMC3011744/ /pubmed/21589487 http://dx.doi.org/10.1107/S1600536810046027 Text en © Chou et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Chou, Wei-Lung
Yih, Kuang-Hway
Lee, Gene-Hsiang
Huang, Yen-Hsiang
Wang, Hsiao-Fen
[(Pyrrolidin-1-yl)carbothio­ylsulfan­yl]methyl pyrrolidine-1-carbodithio­ate
title [(Pyrrolidin-1-yl)carbothio­ylsulfan­yl]methyl pyrrolidine-1-carbodithio­ate
title_full [(Pyrrolidin-1-yl)carbothio­ylsulfan­yl]methyl pyrrolidine-1-carbodithio­ate
title_fullStr [(Pyrrolidin-1-yl)carbothio­ylsulfan­yl]methyl pyrrolidine-1-carbodithio­ate
title_full_unstemmed [(Pyrrolidin-1-yl)carbothio­ylsulfan­yl]methyl pyrrolidine-1-carbodithio­ate
title_short [(Pyrrolidin-1-yl)carbothio­ylsulfan­yl]methyl pyrrolidine-1-carbodithio­ate
title_sort [(pyrrolidin-1-yl)carbothio­ylsulfan­yl]methyl pyrrolidine-1-carbodithio­ate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3011744/
https://www.ncbi.nlm.nih.gov/pubmed/21589487
http://dx.doi.org/10.1107/S1600536810046027
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AT huangyenhsiang pyrrolidin1ylcarbothioylsulfanylmethylpyrrolidine1carbodithioate
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