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Density measurement of samples under high pressure using synchrotron microtomography and diamond anvil cell techniques

Accurate mass density information is critical in high-pressure studies of materials. It is, however, very difficult to measure the mass densities of amorphous materials under high pressure with a diamond anvil cell (DAC). Employing tomography to measure mass density of amorphous samples under high p...

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Detalles Bibliográficos
Autores principales: Xiao, Xianghui, Liu, Haozhe, Wang, Luhong, De Carlo, Francesco
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3025657/
https://www.ncbi.nlm.nih.gov/pubmed/20400834
http://dx.doi.org/10.1107/S0909049510008502
Descripción
Sumario:Accurate mass density information is critical in high-pressure studies of materials. It is, however, very difficult to measure the mass densities of amorphous materials under high pressure with a diamond anvil cell (DAC). Employing tomography to measure mass density of amorphous samples under high pressure in a DAC has recently been reported. In reality, the tomography data of a sample in a DAC suffers from not only noise but also from the missing angle problem owing to the geometry of the DAC. An algorithm that can suppress noise and overcome the missing angle problem has been developed to obtain accurate mass density information from such ill-posed data. The validity of the proposed methods was supported with simulations.