2-(Furan-2-yl)-5-(2-nitro­benz­yl)-2,3-dihydro-1,5-benzothia­zepin-4(5H)-one

The title compound, C(20)H(16)N(2)O(4)S, was prepared by introduction of a 2-nitro­benzyl group to 2-(furan-2-yl)-2,3-dihydro-1,5-benzothia­zepin-4(5H)-one via an alkaline-catalysed reaction. The thia­zepine ring adopts a twist-boat conformation. The furan ring is oriented at dihedral angles of 56.7...

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Detalles Bibliográficos
Autores principales: Huang, Zhao-Hui, Chu, Yong, Ye, De-Yong
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3050135/
https://www.ncbi.nlm.nih.gov/pubmed/21522675
http://dx.doi.org/10.1107/S1600536810052098
Descripción
Sumario:The title compound, C(20)H(16)N(2)O(4)S, was prepared by introduction of a 2-nitro­benzyl group to 2-(furan-2-yl)-2,3-dihydro-1,5-benzothia­zepin-4(5H)-one via an alkaline-catalysed reaction. The thia­zepine ring adopts a twist-boat conformation. The furan ring is oriented at dihedral angles of 56.75 (14) and 10.82 (14)° with respect to the two benzene rings, while the two benzene rings make a dihedral angle of 62.96 (10)°. Weak inter­molecular C—H⋯O hydrogen bonds occur in the crystal structure.

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