2,2′-Bis(meth­oxy­meth­oxy)-3,3′-diphenyl-1,1′-binaphthalene

The asymmetric unit of the title compound, C(36)H(30)O(4), contains two crystallographically independent mol­ecules of similar geometry. In both mol­ecules, the meth­oxy­meth­oxy groups are disordered over two positions with refined site occupancies of 0.613 (3):0.387 (3) and 0.589 (4):0.411 (4). Th...

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Detalles Bibliográficos
Autores principales: Zong, Hua, Huang, Hua-Yin, Hu, Bing, Bian, Guang-Ling, Song, Ling
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3050160/
https://www.ncbi.nlm.nih.gov/pubmed/21522721
http://dx.doi.org/10.1107/S1600536810053018
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author Zong, Hua
Huang, Hua-Yin
Hu, Bing
Bian, Guang-Ling
Song, Ling
author_facet Zong, Hua
Huang, Hua-Yin
Hu, Bing
Bian, Guang-Ling
Song, Ling
author_sort Zong, Hua
collection PubMed
description The asymmetric unit of the title compound, C(36)H(30)O(4), contains two crystallographically independent mol­ecules of similar geometry. In both mol­ecules, the meth­oxy­meth­oxy groups are disordered over two positions with refined site occupancies of 0.613 (3):0.387 (3) and 0.589 (4):0.411 (4). The dihedral angles between the naphthalene planes within the same mol­ecule are 71.72 (7) and 71.73 (8)°. In the crystal, neighbouring mol­ecules are linked by inter­molecular C—H⋯O hydrogen bonds, forming double chains parallel to the c axis.
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spelling pubmed-30501602011-04-26 2,2′-Bis(meth­oxy­meth­oxy)-3,3′-diphenyl-1,1′-binaphthalene Zong, Hua Huang, Hua-Yin Hu, Bing Bian, Guang-Ling Song, Ling Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(36)H(30)O(4), contains two crystallographically independent mol­ecules of similar geometry. In both mol­ecules, the meth­oxy­meth­oxy groups are disordered over two positions with refined site occupancies of 0.613 (3):0.387 (3) and 0.589 (4):0.411 (4). The dihedral angles between the naphthalene planes within the same mol­ecule are 71.72 (7) and 71.73 (8)°. In the crystal, neighbouring mol­ecules are linked by inter­molecular C—H⋯O hydrogen bonds, forming double chains parallel to the c axis. International Union of Crystallography 2010-12-24 /pmc/articles/PMC3050160/ /pubmed/21522721 http://dx.doi.org/10.1107/S1600536810053018 Text en © Zong et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zong, Hua
Huang, Hua-Yin
Hu, Bing
Bian, Guang-Ling
Song, Ling
2,2′-Bis(meth­oxy­meth­oxy)-3,3′-diphenyl-1,1′-binaphthalene
title 2,2′-Bis(meth­oxy­meth­oxy)-3,3′-diphenyl-1,1′-binaphthalene
title_full 2,2′-Bis(meth­oxy­meth­oxy)-3,3′-diphenyl-1,1′-binaphthalene
title_fullStr 2,2′-Bis(meth­oxy­meth­oxy)-3,3′-diphenyl-1,1′-binaphthalene
title_full_unstemmed 2,2′-Bis(meth­oxy­meth­oxy)-3,3′-diphenyl-1,1′-binaphthalene
title_short 2,2′-Bis(meth­oxy­meth­oxy)-3,3′-diphenyl-1,1′-binaphthalene
title_sort 2,2′-bis(meth­oxy­meth­oxy)-3,3′-diphenyl-1,1′-binaphthalene
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3050160/
https://www.ncbi.nlm.nih.gov/pubmed/21522721
http://dx.doi.org/10.1107/S1600536810053018
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AT hubing 22bismethoxymethoxy33diphenyl11binaphthalene
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AT songling 22bismethoxymethoxy33diphenyl11binaphthalene

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