2,3-Dibromo-1-(4-methyl­phen­yl)-3-(5-nitro­furan-2-yl)propan-1-one

In the title compound, C(14)H(11)Br(2)NO(4), the whole mol­ecule is disordered over two positions with a refined occupancy ratio of 0.539 (9):0.461 (9). The 2-nitro­furan and toluene groups are approximately planar, with maximum deviations of 0.176 (11) and 0.121 (14) Å, respectively, in the major c...

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Detalles Bibliográficos
Autores principales: Fun, Hoong-Kun, Shahani, Tara, Nithinchandra, Kalluraya, Balakrishna
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3050337/
https://www.ncbi.nlm.nih.gov/pubmed/21522790
http://dx.doi.org/10.1107/S1600536810050488
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author Fun, Hoong-Kun
Shahani, Tara
Nithinchandra,
Kalluraya, Balakrishna
author_facet Fun, Hoong-Kun
Shahani, Tara
Nithinchandra,
Kalluraya, Balakrishna
author_sort Fun, Hoong-Kun
collection PubMed
description In the title compound, C(14)H(11)Br(2)NO(4), the whole mol­ecule is disordered over two positions with a refined occupancy ratio of 0.539 (9):0.461 (9). The 2-nitro­furan and toluene groups are approximately planar, with maximum deviations of 0.176 (11) and 0.121 (14) Å, respectively, in the major component and 0.208 (11) and 0.30 (17) Å in the minor component. The dihedral angles between the 2-nitro­furan and toluene groups are 8.7 (5) and 8.0 (9)° for the major and minor components, respectively. In the crystal, weak inter­molecular C—H⋯O inter­actions connect mol­ecules into a three-dimensional network, generating R (2) (1)(6) ring motifs.
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spelling pubmed-30503372011-04-26 2,3-Dibromo-1-(4-methyl­phen­yl)-3-(5-nitro­furan-2-yl)propan-1-one Fun, Hoong-Kun Shahani, Tara Nithinchandra, Kalluraya, Balakrishna Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(14)H(11)Br(2)NO(4), the whole mol­ecule is disordered over two positions with a refined occupancy ratio of 0.539 (9):0.461 (9). The 2-nitro­furan and toluene groups are approximately planar, with maximum deviations of 0.176 (11) and 0.121 (14) Å, respectively, in the major component and 0.208 (11) and 0.30 (17) Å in the minor component. The dihedral angles between the 2-nitro­furan and toluene groups are 8.7 (5) and 8.0 (9)° for the major and minor components, respectively. In the crystal, weak inter­molecular C—H⋯O inter­actions connect mol­ecules into a three-dimensional network, generating R (2) (1)(6) ring motifs. International Union of Crystallography 2010-12-11 /pmc/articles/PMC3050337/ /pubmed/21522790 http://dx.doi.org/10.1107/S1600536810050488 Text en © Fun et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Fun, Hoong-Kun
Shahani, Tara
Nithinchandra,
Kalluraya, Balakrishna
2,3-Dibromo-1-(4-methyl­phen­yl)-3-(5-nitro­furan-2-yl)propan-1-one
title 2,3-Dibromo-1-(4-methyl­phen­yl)-3-(5-nitro­furan-2-yl)propan-1-one
title_full 2,3-Dibromo-1-(4-methyl­phen­yl)-3-(5-nitro­furan-2-yl)propan-1-one
title_fullStr 2,3-Dibromo-1-(4-methyl­phen­yl)-3-(5-nitro­furan-2-yl)propan-1-one
title_full_unstemmed 2,3-Dibromo-1-(4-methyl­phen­yl)-3-(5-nitro­furan-2-yl)propan-1-one
title_short 2,3-Dibromo-1-(4-methyl­phen­yl)-3-(5-nitro­furan-2-yl)propan-1-one
title_sort 2,3-dibromo-1-(4-methyl­phen­yl)-3-(5-nitro­furan-2-yl)propan-1-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3050337/
https://www.ncbi.nlm.nih.gov/pubmed/21522790
http://dx.doi.org/10.1107/S1600536810050488
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AT kallurayabalakrishna 23dibromo14methylphenyl35nitrofuran2ylpropan1one

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