(S)-N-Benzyl-2-methyl-1,2,3,4-tetra­hydro­isoquinoline-3-carboxamide

The structure of the title compound, C(18)H(20)N(2)O, at 173 K has hexa­gonal (P6(1)) symmetry. The N-containing six-membered ring assumes a half-chair conformation. In the crystal, inter­molecular N—H⋯O hydrogen bonding via the amide groups cross-link the mol­ecules along the a axis. The absolute c...

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Detalles Bibliográficos
Autores principales: Naicker, Tricia, Govender, Thavendran, Kruger, Hendrik. G., Maguire, Glenn. E.M.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3050362/
https://www.ncbi.nlm.nih.gov/pubmed/21522778
http://dx.doi.org/10.1107/S1600536810050361
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author Naicker, Tricia
Govender, Thavendran
Kruger, Hendrik. G.
Maguire, Glenn. E.M.
author_facet Naicker, Tricia
Govender, Thavendran
Kruger, Hendrik. G.
Maguire, Glenn. E.M.
author_sort Naicker, Tricia
collection PubMed
description The structure of the title compound, C(18)H(20)N(2)O, at 173 K has hexa­gonal (P6(1)) symmetry. The N-containing six-membered ring assumes a half-chair conformation. In the crystal, inter­molecular N—H⋯O hydrogen bonding via the amide groups cross-link the mol­ecules along the a axis. The absolute configuration was confirmed by 2D NMR studies.
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spelling pubmed-30503622011-04-26 (S)-N-Benzyl-2-methyl-1,2,3,4-tetra­hydro­isoquinoline-3-carboxamide Naicker, Tricia Govender, Thavendran Kruger, Hendrik. G. Maguire, Glenn. E.M. Acta Crystallogr Sect E Struct Rep Online Organic Papers The structure of the title compound, C(18)H(20)N(2)O, at 173 K has hexa­gonal (P6(1)) symmetry. The N-containing six-membered ring assumes a half-chair conformation. In the crystal, inter­molecular N—H⋯O hydrogen bonding via the amide groups cross-link the mol­ecules along the a axis. The absolute configuration was confirmed by 2D NMR studies. International Union of Crystallography 2010-12-11 /pmc/articles/PMC3050362/ /pubmed/21522778 http://dx.doi.org/10.1107/S1600536810050361 Text en © Naicker et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Naicker, Tricia
Govender, Thavendran
Kruger, Hendrik. G.
Maguire, Glenn. E.M.
(S)-N-Benzyl-2-methyl-1,2,3,4-tetra­hydro­isoquinoline-3-carboxamide
title (S)-N-Benzyl-2-methyl-1,2,3,4-tetra­hydro­isoquinoline-3-carboxamide
title_full (S)-N-Benzyl-2-methyl-1,2,3,4-tetra­hydro­isoquinoline-3-carboxamide
title_fullStr (S)-N-Benzyl-2-methyl-1,2,3,4-tetra­hydro­isoquinoline-3-carboxamide
title_full_unstemmed (S)-N-Benzyl-2-methyl-1,2,3,4-tetra­hydro­isoquinoline-3-carboxamide
title_short (S)-N-Benzyl-2-methyl-1,2,3,4-tetra­hydro­isoquinoline-3-carboxamide
title_sort (s)-n-benzyl-2-methyl-1,2,3,4-tetra­hydro­isoquinoline-3-carboxamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3050362/
https://www.ncbi.nlm.nih.gov/pubmed/21522778
http://dx.doi.org/10.1107/S1600536810050361
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AT maguireglennem snbenzyl2methyl1234tetrahydroisoquinoline3carboxamide

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