1-[4-(3-{[5-(4-Chloro­phen­yl)furan-2-yl]methyl­idene­amino}-2,5-dioxoimidazol­idin-1-yl)but­yl]-4-methyl­piperazine-1,4-diium dichloride hemihydrate

The title compound, C(23)H(30)ClN(5)O(3) (2+)·2Cl(−)·0.5H(2)O, was synthesized by N-alkyl­ation of 1-({[5-(4-chloro­phen­yl)-2-furan­yl]methyl­ene}amino)-2,4-imidazolidinedione with 1-bromo-4-chloro­butane, and N-methyl­piperazine. In the crystal, the cations, anions and water mol­ecules are linked...

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Detalles Bibliográficos
Autores principales: Liang, Yan-Shu, Mu, Shuai, Liu, Ying, Liu, Deng-Ke
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3051443/
https://www.ncbi.nlm.nih.gov/pubmed/21523006
http://dx.doi.org/10.1107/S1600536811000560
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author Liang, Yan-Shu
Mu, Shuai
Liu, Ying
Liu, Deng-Ke
author_facet Liang, Yan-Shu
Mu, Shuai
Liu, Ying
Liu, Deng-Ke
author_sort Liang, Yan-Shu
collection PubMed
description The title compound, C(23)H(30)ClN(5)O(3) (2+)·2Cl(−)·0.5H(2)O, was synthesized by N-alkyl­ation of 1-({[5-(4-chloro­phen­yl)-2-furan­yl]methyl­ene}amino)-2,4-imidazolidinedione with 1-bromo-4-chloro­butane, and N-methyl­piperazine. In the crystal, the cations, anions and water mol­ecules are linked by O—H⋯Cl and N—H⋯Cl hydrogen bonds.
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spelling pubmed-30514432011-04-26 1-[4-(3-{[5-(4-Chloro­phen­yl)furan-2-yl]methyl­idene­amino}-2,5-dioxoimidazol­idin-1-yl)but­yl]-4-methyl­piperazine-1,4-diium dichloride hemihydrate Liang, Yan-Shu Mu, Shuai Liu, Ying Liu, Deng-Ke Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(23)H(30)ClN(5)O(3) (2+)·2Cl(−)·0.5H(2)O, was synthesized by N-alkyl­ation of 1-({[5-(4-chloro­phen­yl)-2-furan­yl]methyl­ene}amino)-2,4-imidazolidinedione with 1-bromo-4-chloro­butane, and N-methyl­piperazine. In the crystal, the cations, anions and water mol­ecules are linked by O—H⋯Cl and N—H⋯Cl hydrogen bonds. International Union of Crystallography 2011-01-12 /pmc/articles/PMC3051443/ /pubmed/21523006 http://dx.doi.org/10.1107/S1600536811000560 Text en © Liang et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Liang, Yan-Shu
Mu, Shuai
Liu, Ying
Liu, Deng-Ke
1-[4-(3-{[5-(4-Chloro­phen­yl)furan-2-yl]methyl­idene­amino}-2,5-dioxoimidazol­idin-1-yl)but­yl]-4-methyl­piperazine-1,4-diium dichloride hemihydrate
title 1-[4-(3-{[5-(4-Chloro­phen­yl)furan-2-yl]methyl­idene­amino}-2,5-dioxoimidazol­idin-1-yl)but­yl]-4-methyl­piperazine-1,4-diium dichloride hemihydrate
title_full 1-[4-(3-{[5-(4-Chloro­phen­yl)furan-2-yl]methyl­idene­amino}-2,5-dioxoimidazol­idin-1-yl)but­yl]-4-methyl­piperazine-1,4-diium dichloride hemihydrate
title_fullStr 1-[4-(3-{[5-(4-Chloro­phen­yl)furan-2-yl]methyl­idene­amino}-2,5-dioxoimidazol­idin-1-yl)but­yl]-4-methyl­piperazine-1,4-diium dichloride hemihydrate
title_full_unstemmed 1-[4-(3-{[5-(4-Chloro­phen­yl)furan-2-yl]methyl­idene­amino}-2,5-dioxoimidazol­idin-1-yl)but­yl]-4-methyl­piperazine-1,4-diium dichloride hemihydrate
title_short 1-[4-(3-{[5-(4-Chloro­phen­yl)furan-2-yl]methyl­idene­amino}-2,5-dioxoimidazol­idin-1-yl)but­yl]-4-methyl­piperazine-1,4-diium dichloride hemihydrate
title_sort 1-[4-(3-{[5-(4-chloro­phen­yl)furan-2-yl]methyl­idene­amino}-2,5-dioxoimidazol­idin-1-yl)but­yl]-4-methyl­piperazine-1,4-diium dichloride hemihydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3051443/
https://www.ncbi.nlm.nih.gov/pubmed/21523006
http://dx.doi.org/10.1107/S1600536811000560
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AT liudengke 14354chlorophenylfuran2ylmethylideneamino25dioxoimidazolidin1ylbutyl4methylpiperazine14diiumdichloridehemihydrate

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