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3-Hydroxy-N′-[(E)-2-thienylmethylidene]-2-naphthohydrazide
The asymmetric unit of the title compound, C(16)H(12)N(2)O(2)S, contains three independent molecules. Intramolecular N—H⋯O hydrogen bonds in the three molecules lead to very similar conformations: the thiopene ring and naphthalene ring system in the three molecules form dihedral angles of 10.3 ...
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Formato: | Texto |
Lenguaje: | English |
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International Union of Crystallography
2011
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3051446/ https://www.ncbi.nlm.nih.gov/pubmed/21522969 http://dx.doi.org/10.1107/S160053681005405X |
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author | Wu, Qingkun Yin, Handong Wang, Daqi |
author_facet | Wu, Qingkun Yin, Handong Wang, Daqi |
author_sort | Wu, Qingkun |
collection | PubMed |
description | The asymmetric unit of the title compound, C(16)H(12)N(2)O(2)S, contains three independent molecules. Intramolecular N—H⋯O hydrogen bonds in the three molecules lead to very similar conformations: the thiopene ring and naphthalene ring system in the three molecules form dihedral angles of 10.3 (2), 9.1 (2) and 9.3 (3)°. In the crystal structure, intermolecular O—H⋯O hydrogen bonds link the molecules into chains propagating in [031]. |
format | Text |
id | pubmed-3051446 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2011 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-30514462011-04-26 3-Hydroxy-N′-[(E)-2-thienylmethylidene]-2-naphthohydrazide Wu, Qingkun Yin, Handong Wang, Daqi Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(16)H(12)N(2)O(2)S, contains three independent molecules. Intramolecular N—H⋯O hydrogen bonds in the three molecules lead to very similar conformations: the thiopene ring and naphthalene ring system in the three molecules form dihedral angles of 10.3 (2), 9.1 (2) and 9.3 (3)°. In the crystal structure, intermolecular O—H⋯O hydrogen bonds link the molecules into chains propagating in [031]. International Union of Crystallography 2011-01-08 /pmc/articles/PMC3051446/ /pubmed/21522969 http://dx.doi.org/10.1107/S160053681005405X Text en © Wu et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Wu, Qingkun Yin, Handong Wang, Daqi 3-Hydroxy-N′-[(E)-2-thienylmethylidene]-2-naphthohydrazide |
title | 3-Hydroxy-N′-[(E)-2-thienylmethylidene]-2-naphthohydrazide |
title_full | 3-Hydroxy-N′-[(E)-2-thienylmethylidene]-2-naphthohydrazide |
title_fullStr | 3-Hydroxy-N′-[(E)-2-thienylmethylidene]-2-naphthohydrazide |
title_full_unstemmed | 3-Hydroxy-N′-[(E)-2-thienylmethylidene]-2-naphthohydrazide |
title_short | 3-Hydroxy-N′-[(E)-2-thienylmethylidene]-2-naphthohydrazide |
title_sort | 3-hydroxy-n′-[(e)-2-thienylmethylidene]-2-naphthohydrazide |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3051446/ https://www.ncbi.nlm.nih.gov/pubmed/21522969 http://dx.doi.org/10.1107/S160053681005405X |
work_keys_str_mv | AT wuqingkun 3hydroxyne2thienylmethylidene2naphthohydrazide AT yinhandong 3hydroxyne2thienylmethylidene2naphthohydrazide AT wangdaqi 3hydroxyne2thienylmethylidene2naphthohydrazide |