2-(4-Meth­oxy­phen­yl)-4H-1,3,2-benzoxathia­phosphinine 2-sulfide

The asymmetric unit of the title compound, C(14)H(13)O(2)PS(2), contains two crystallographically independent mol­ecules, which differ in the conformation of the 1,3,2-benzoxathia­phosphinine moieties (screw boat in the first mol­ecule and envelope in the second mol­ecule). In the crystal, neither c...

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Detalles Bibliográficos
Autores principales: Osyanin, Vitaly A., Ivleva, Elena A., Rybakov, Victor B., Klimochkin, Yurij N.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3051562/
https://www.ncbi.nlm.nih.gov/pubmed/21523063
http://dx.doi.org/10.1107/S1600536810053146
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author Osyanin, Vitaly A.
Ivleva, Elena A.
Rybakov, Victor B.
Klimochkin, Yurij N.
author_facet Osyanin, Vitaly A.
Ivleva, Elena A.
Rybakov, Victor B.
Klimochkin, Yurij N.
author_sort Osyanin, Vitaly A.
collection PubMed
description The asymmetric unit of the title compound, C(14)H(13)O(2)PS(2), contains two crystallographically independent mol­ecules, which differ in the conformation of the 1,3,2-benzoxathia­phosphinine moieties (screw boat in the first mol­ecule and envelope in the second mol­ecule). In the crystal, neither classical nor non-classical hydrogen bonds are found. Weak inter­actions (about 2.9–3.0 Å) between the lone pair of the terminal S atoms with H atoms occur. This compound was further characterized by (1)H NMR and IR spectroscopy.
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spelling pubmed-30515622011-04-26 2-(4-Meth­oxy­phen­yl)-4H-1,3,2-benzoxathia­phosphinine 2-sulfide Osyanin, Vitaly A. Ivleva, Elena A. Rybakov, Victor B. Klimochkin, Yurij N. Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(14)H(13)O(2)PS(2), contains two crystallographically independent mol­ecules, which differ in the conformation of the 1,3,2-benzoxathia­phosphinine moieties (screw boat in the first mol­ecule and envelope in the second mol­ecule). In the crystal, neither classical nor non-classical hydrogen bonds are found. Weak inter­actions (about 2.9–3.0 Å) between the lone pair of the terminal S atoms with H atoms occur. This compound was further characterized by (1)H NMR and IR spectroscopy. International Union of Crystallography 2011-01-15 /pmc/articles/PMC3051562/ /pubmed/21523063 http://dx.doi.org/10.1107/S1600536810053146 Text en © Osyanin et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Osyanin, Vitaly A.
Ivleva, Elena A.
Rybakov, Victor B.
Klimochkin, Yurij N.
2-(4-Meth­oxy­phen­yl)-4H-1,3,2-benzoxathia­phosphinine 2-sulfide
title 2-(4-Meth­oxy­phen­yl)-4H-1,3,2-benzoxathia­phosphinine 2-sulfide
title_full 2-(4-Meth­oxy­phen­yl)-4H-1,3,2-benzoxathia­phosphinine 2-sulfide
title_fullStr 2-(4-Meth­oxy­phen­yl)-4H-1,3,2-benzoxathia­phosphinine 2-sulfide
title_full_unstemmed 2-(4-Meth­oxy­phen­yl)-4H-1,3,2-benzoxathia­phosphinine 2-sulfide
title_short 2-(4-Meth­oxy­phen­yl)-4H-1,3,2-benzoxathia­phosphinine 2-sulfide
title_sort 2-(4-meth­oxy­phen­yl)-4h-1,3,2-benzoxathia­phosphinine 2-sulfide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3051562/
https://www.ncbi.nlm.nih.gov/pubmed/21523063
http://dx.doi.org/10.1107/S1600536810053146
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AT rybakovvictorb 24methoxyphenyl4h132benzoxathiaphosphinine2sulfide
AT klimochkinyurijn 24methoxyphenyl4h132benzoxathiaphosphinine2sulfide

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